N-(2-hydroxypropyl)-N-[(2-methoxyimino)ethyl]-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(2-hydroxypropyl)-N-[(2-methoxyimino)ethyl]-4-methylbenzenesulfonamide
CAS No.:300547-85-7
Molecular Formula:C₁₃H₂₀N₂O₄S
Molecular Weight:300.379
Hs Code.:

Synonyms:N-(2-hydroxypropyl)-N-[(2-methoxyimino)ethyl]-4-methylbenzenesulfonamide

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Chemical Property of N-(2-hydroxypropyl)-N-[(2-methoxyimino)ethyl]-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of N-(2-hydroxypropyl)-N-[(2-methoxyimino)ethyl]-4-methylbenzenesulfonamide

There total 1 articles about N-(2-hydroxypropyl)-N-[(2-methoxyimino)ethyl]-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: (2-hydroxy-propylamino)-acetaldehyde O-methyl-oxime

: 300547-85-7
N-(2-hydroxypropyl)-N-[(2-methoxyimino)ethyl]-4-methylbenzenesulfonamide

Guidance literature:: With sodium carbonate; In water; acetone; at 20 ℃; for 3h;
DOI:10.1016/S0040-4020(00)00545-7

Reference yield: 64.0%

: 300547-85-7
N-(2-hydroxypropyl)-N-[(2-methoxyimino)ethyl]-4-methylbenzenesulfonamide

: 300547-89-1
N-[(2-methoxyimino)ethyl]-4-methyl-N-(2-oxopropyl)benzenesulfonamide

Guidance literature:: With pyridine; chromium(VI) oxide; In dichloromethane; at 20 ℃;
DOI:10.1016/S0040-4020(00)00545-7

Reference yield:

: 300547-85-7
N-(2-hydroxypropyl)-N-[(2-methoxyimino)ethyl]-4-methylbenzenesulfonamide

: 178624-90-3
(3S)-3-methyl-1-[(4-methylbenzene)sulfonyl]piperazine

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / CrO₃; pyridine / CH₂Cl₂ / 20 °C

2: AIBN; Bu₃SnH / hexane / 5 h / Heating

3: 21 percent / Red-Al / benzene; toluene / Heating

With pyridine; chromium(VI) oxide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium bis(2-methoxyethoxy)aluminium dihydride; In hexane; dichloromethane; toluene; benzene; 1: Oxidation / 2: Cyclization / 3: Reduction;
DOI:10.1016/S0040-4020(00)00545-7