2-methoxymethoxyphenylboronic acid MIDA ester

Base Information

• Chemical Name: 2-methoxymethoxyphenylboronic acid MIDA ester
• CAS No.: 1613586-42-7
• Molecular Formula: C₁₃H₁₆BNO₆
• Molecular Weight: 293.084
• Mol file: 1613586-42-7.mol

Synonyms:2-methoxymethoxyphenylboronic acid MIDA ester

Chemical Property of 2-methoxymethoxyphenylboronic acid MIDA ester

Chemical Property:

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Technology Process of 2-methoxymethoxyphenylboronic acid MIDA ester

There total 1 articles about 2-methoxymethoxyphenylboronic acid MIDA ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N-methyliminodiacetic acid (4408-64-4) + ortho-methoxymethyleneoxyphenylboronic acid (115377-93-0) → 2-methoxymethoxyphenylboronic acid MIDA ester (1613586-42-7)

Guidance literature:

In N,N-dimethyl-formamide; at 120 ℃; for 3h; Inert atmosphere; Molecular sieve;

DOI:10.1002/adsc.201301023

Reference yield: 95.0%

2-methoxymethoxyphenylboronic acid MIDA ester (1613586-42-7) → 2-hydroxyphenylboronic acid MIDA ester (1613586-35-8)

Guidance literature:

With chloro-trimethyl-silane; In dichloromethane; acetonitrile; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1002/adsc.201301023

upstream raw materials:

N-methyliminodiacetic acid

ortho-methoxymethyleneoxyphenylboronic acid

Downstream raw materials:

2-hydroxyphenylboronic acid MIDA ester

Refernces