Technology Process of C34H33NO3
There total 3 articles about C34H33NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-(1-adamantyl)-4-bromophenol;
With
palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium acetate; bis(pinacol)diborane;
In
1,4-dioxane;
for 2h;
Reflux;
Inert atmosphere;
6-bromonaphthalene-2-carboxylic acid benzyloxyamide;
With
sodium carbonate;
In
1,4-dioxane;
for 2h;
Reflux;
Inert atmosphere;
DOI:10.1016/j.ejmech.2014.04.021
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hydroxide / methanol / 1 h
2.1: bis(pinacol)diborane; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium acetate / 1,4-dioxane / 2 h / Reflux; Inert atmosphere
2.2: 2 h / Reflux; Inert atmosphere
With
palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium acetate; bis(pinacol)diborane; potassium hydroxide;
In
1,4-dioxane; methanol;
2.1: |Suzuki Coupling / 2.2: |Suzuki Coupling;
DOI:10.1016/j.ejmech.2014.04.021
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / tetrahydrofuran / 0.17 h / 0 °C
2.1: potassium hydroxide / methanol / 1 h
3.1: bis(pinacol)diborane; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium acetate / 1,4-dioxane / 2 h / Reflux; Inert atmosphere
3.2: 2 h / Reflux; Inert atmosphere
With
palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium acetate; triethylamine; bis(pinacol)diborane; potassium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol;
3.1: |Suzuki Coupling / 3.2: |Suzuki Coupling;
DOI:10.1016/j.ejmech.2014.04.021
