6-bromonaphthalene-2-carboxylic acid benzyloxyamide

Base Information

Chemical Name:6-bromonaphthalene-2-carboxylic acid benzyloxyamide
CAS No.:1609552-91-1
Molecular Formula:C₁₈H₁₄BrNO₂
Molecular Weight:356.219
Hs Code.:

Synonyms:6-bromonaphthalene-2-carboxylic acid benzyloxyamide

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Chemical Property of 6-bromonaphthalene-2-carboxylic acid benzyloxyamide

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Technology Process of 6-bromonaphthalene-2-carboxylic acid benzyloxyamide

There total 2 articles about 6-bromonaphthalene-2-carboxylic acid benzyloxyamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 622-33-3
N-benzyloxyamine

: C₁₄H₁₁BrO₃

: 1609552-91-1
6-bromonaphthalene-2-carboxylic acid benzyloxyamide

Guidance literature:: With potassium hydroxide; In methanol; for 1h;
DOI:10.1016/j.ejmech.2014.04.021

Reference yield:

: 5773-80-8
6-bromo-2-naphthoic acid

: 1609552-91-1
6-bromonaphthalene-2-carboxylic acid benzyloxyamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 0.17 h / 0 °C

2: potassium hydroxide / methanol / 1 h

With triethylamine; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.ejmech.2014.04.021

Reference yield: 28.0%

: 1609552-91-1
6-bromonaphthalene-2-carboxylic acid benzyloxyamide

: 104224-68-2
2-(1-adamantyl)-4-bromophenol

: 1609552-93-3
C₃₄H₃₃NO₃

Guidance literature:: 2-(1-adamantyl)-4-bromophenol; With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium acetate; bis(pinacol)diborane; In 1,4-dioxane; for 2h; Reflux; Inert atmosphere;

6-bromonaphthalene-2-carboxylic acid benzyloxyamide; With sodium carbonate; In 1,4-dioxane; for 2h; Reflux; Inert atmosphere;
DOI:10.1016/j.ejmech.2014.04.021