N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine methyl ester

Base Information

Chemical Name:N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine methyl ester
CAS No.:1334648-27-9
Molecular Formula:C₃₆H₄₁N₃O₄
Molecular Weight:579.739
Hs Code.:

Synonyms:N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine methyl ester

Suppliers and Price of N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine methyl ester

There total 8 articles about N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 937801-67-7
methyl-N^α-(((9H-fluoren-9-yl)methoxy)carbonyl)-N^τ-trityl-L-histidinate

: C₁₅H₂₁F₃O₃S

: 1334648-27-9
N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine methyl ester

Guidance literature:: In dichloromethane; at -75 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo201599c

Reference yield:

: C₅₅H₅₆N₃O₄⁽¹⁺⁾

: 1334648-27-9
N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine methyl ester

Guidance literature:: With chlorotriisopropylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2013.02.020

Reference yield:

: 10472-97-6
8-phenyloctan-1-ol

: 1334648-27-9
N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / -75 °C / Inert atmosphere

2: dichloromethane / -75 - 20 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jo201599c