N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine

Base Information

Chemical Name:N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine
CAS No.:1334648-24-6
Molecular Formula:C₃₅H₃₉N₃O₄
Molecular Weight:565.712
Hs Code.:

Synonyms:N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine

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Chemical Property of N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine

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Technology Process of N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine

There total 15 articles about N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: C₂₀H₂₉N₃O₂*(x)ClH

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 1334648-24-6
N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; water; at 20 ℃;
DOI:10.1021/jo201599c

Reference yield: 80.0%

: 1334648-27-9
N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine methyl ester

: 1334648-24-6
N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine

Guidance literature:: N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine methyl ester; With lithium iodide; In ethyl acetate; for 20h; Inert atmosphere; Reflux;

With hydrogenchloride; In water; ethyl acetate;
DOI:10.1021/jo201599c

Reference yield:

: 1334648-21-3
N(α)-[(1,1-dimethylethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine methyl ester

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 1334648-24-6
N(α)-[(9H-fluoren-9-ylmethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine

Guidance literature:: N(α)-[(1,1-dimethylethoxy)carbonyl]-N(?)-(8-phenyloctyl)-L-histidine methyl ester; With lithium hydroxide monohydrate; water; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1h;

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide;