(2R,3S,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-carbaldehyde O-(4-methoxy-benzyl)-oxime

Base Information

Chemical Name:(2R,3S,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-carbaldehyde O-(4-methoxy-benzyl)-oxime
CAS No.:365278-79-1
Molecular Formula:C₁₄H₁₉NO₆
Molecular Weight:297.308
Hs Code.:

Synonyms:(2R,3S,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-carbaldehyde O-(4-methoxy-benzyl)-oxime

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Chemical Property of (2R,3S,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-carbaldehyde O-(4-methoxy-benzyl)-oxime

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Technology Process of (2R,3S,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-carbaldehyde O-(4-methoxy-benzyl)-oxime

There total 3 articles about (2R,3S,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-carbaldehyde O-(4-methoxy-benzyl)-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: O-(4-methoxybenzyl)-hydroxylamine HCl

: 495-75-0
2,5-anhydro-D-mannose

: 365278-79-1
(2R,3S,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-carbaldehyde O-(4-methoxy-benzyl)-oxime

Guidance literature:: In acetate buffer; at 20 ℃; for 0.333333h; pH=4;
DOI:10.1016/S0008-6215(01)00115-X

Reference yield:

: 2014-61-1
N-(4-methoxybenzyloxy)phthalimide

: 365278-79-1
(2R,3S,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-carbaldehyde O-(4-methoxy-benzyl)-oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / hydrazine hydrate; HCl / methanol / 3 h / 20 °C

2: 100 percent / acetate buffer / 0.33 h / 20 °C / pH 4

With hydrogenchloride; hydrazine hydrate; In methanol; acetate buffer;
DOI:10.1016/S0008-6215(01)00115-X

Reference yield:

: 105-13-5
4-Methoxybenzyl alcohol

: 365278-79-1
(2R,3S,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-carbaldehyde O-(4-methoxy-benzyl)-oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / PPh₃; DEAD / tetrahydrofuran / 20 °C

2: 64 percent / hydrazine hydrate; HCl / methanol / 3 h / 20 °C

3: 100 percent / acetate buffer / 0.33 h / 20 °C / pH 4

With hydrogenchloride; hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; acetate buffer;
DOI:10.1016/S0008-6215(01)00115-X