C₃₉H₅₄N₂O₇Si

Base Information

Chemical Name:C₃₉H₅₄N₂O₇Si
CAS No.:910558-57-5
Molecular Formula:C₃₉H₅₄N₂O₇Si
Molecular Weight:690.952
Hs Code.:

C<sub>39</sub>H<sub>54</sub>N<sub>2</sub>O<sub>7</sub>Si

Synonyms:C₃₉H₅₄N₂O₇Si

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Chemical Property of C₃₉H₅₄N₂O₇Si

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Technology Process of C₃₉H₅₄N₂O₇Si

There total 11 articles about C₃₉H₅₄N₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 910558-55-3
C₃₀H₃₄N₂O₆

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 910558-57-5
C₃₉H₅₄N₂O₇Si

Guidance literature:: C₃₀H₃₄N₂O₆; With bis-trimethylsilanyl peroxide; lithium diisopropyl amide; In tetrahydrofuran; at -40 ℃; for 4h;

triisopropylsilyl trifluoromethanesulfonate; In tetrahydrofuran; at -40 - 20 ℃; for 2h;
DOI:10.1021/ol051975x

Reference yield:

: 202807-44-1
6-methoxy-1-methyl-1H-indole-3-carbaldehyde

: 910558-57-5
C₃₉H₅₄N₂O₇Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: 99 percent / NH₄OAc / 1 h / Heating

2.1: 96 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

3.1: ethanol / 25 °C

3.2: 64 percent / N₂H₄*H₂O / ethanol / 5 h / Heating

4.1: 61 percent / EDCI; DMAP / CH₂Cl₂ / 19 h / 25 °C

5.1: 67 percent / p-toluenesulfonyl chloride; Et₃N / CH₂Cl₂ / 20 h / 25 °C

6.1: 96 percent / EDCI; DMAP / CH₂Cl₂ / 16 h / 0 - 25 °C

7.1: 53 percent / various solvent(s) / 90 h / 230 °C

8.1: Chiracel OD / propan-2-ol; hexane

9.1: LDA; bis(trimethylsilyl)peroxide / tetrahydrofuran / 4 h / -40 °C

9.2: 64 percent / tetrahydrofuran / 2 h / -40 - 20 °C

With dmap; lithium aluminium tetrahydride; bis-trimethylsilanyl peroxide; Chiracel OD; ammonium acetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; p-toluenesulfonyl chloride; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane; isopropyl alcohol;
DOI:10.1021/ol051975x

Reference yield:

: 6-methoxy-1-methyl-3-(2-nitrovinyl)-1H-indole

: 910558-57-5
C₃₉H₅₄N₂O₇Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 96 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

2.1: ethanol / 25 °C

2.2: 64 percent / N₂H₄*H₂O / ethanol / 5 h / Heating

3.1: 61 percent / EDCI; DMAP / CH₂Cl₂ / 19 h / 25 °C

4.1: 67 percent / p-toluenesulfonyl chloride; Et₃N / CH₂Cl₂ / 20 h / 25 °C

5.1: 96 percent / EDCI; DMAP / CH₂Cl₂ / 16 h / 0 - 25 °C

6.1: 53 percent / various solvent(s) / 90 h / 230 °C

7.1: Chiracel OD / propan-2-ol; hexane

8.1: LDA; bis(trimethylsilyl)peroxide / tetrahydrofuran / 4 h / -40 °C

8.2: 64 percent / tetrahydrofuran / 2 h / -40 - 20 °C

With dmap; lithium aluminium tetrahydride; bis-trimethylsilanyl peroxide; Chiracel OD; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; p-toluenesulfonyl chloride; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane; isopropyl alcohol;
DOI:10.1021/ol051975x