tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)-N-(trifluoroacetyl)glycinate

Base Information

Chemical Name:tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)-N-(trifluoroacetyl)glycinate
CAS No.:1427753-06-7
Molecular Formula:C₂₀H₂₈F₃N₃O₇S
Molecular Weight:511.519
Hs Code.:

Synonyms:tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)-N-(trifluoroacetyl)glycinate

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Chemical Property of tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)-N-(trifluoroacetyl)glycinate

Chemical Property:

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Technology Process of tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)-N-(trifluoroacetyl)glycinate

There total 3 articles about tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)-N-(trifluoroacetyl)glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1427753-05-6
tert-butyl N-(3-aminobenzyl)-N-(trifluoroacetyl)glycinate

: 147000-89-3
N-tert-butyloxycarbonylsulfamoyl chloride

: 1427753-06-7
tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)-N-(trifluoroacetyl)glycinate

Guidance literature:: With triethylamine; In hexane; dichloromethane; water; ethyl acetate;

Reference yield:

: 943741-89-7
tert-butyl N-(3-nitrobenzyl)glycinate

: 1427753-06-7
tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)-N-(trifluoroacetyl)glycinate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 4 h / 20 °C / Cooling with ice

2: iron; ammonium chloride / water; ethanol / 1 h / 100 °C

3: triethylamine / dichloromethane; water; ethyl acetate; hexane

With iron; ammonium chloride; triethylamine; In ethanol; hexane; dichloromethane; water; ethyl acetate;

Reference yield:

: 943741-88-6
tert-butyl N-(3-nitrobenzyl)-N-(trifluoroacetyl)glycinate

: 1427753-06-7
tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)-N-(trifluoroacetyl)glycinate

Guidance literature:: Multi-step reaction with 2 steps

1: iron; ammonium chloride / water; ethanol / 1 h / 100 °C

2: triethylamine / dichloromethane; water; ethyl acetate; hexane

With iron; ammonium chloride; triethylamine; In ethanol; hexane; dichloromethane; water; ethyl acetate;