tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)glycinate

Base Information

Chemical Name:tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)glycinate
CAS No.:1427753-07-8
Molecular Formula:C₁₈H₂₉N₃O₆S
Molecular Weight:415.511
Hs Code.:

Synonyms:tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)glycinate

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Chemical Property of tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)glycinate

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Technology Process of tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)glycinate

There total 4 articles about tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1427753-06-7
tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)-N-(trifluoroacetyl)glycinate

: 1427753-07-8
tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)glycinate

Guidance literature:: With potassium carbonate; In water; at 20 ℃; for 5h;

Reference yield:

: 1427753-05-6
tert-butyl N-(3-aminobenzyl)-N-(trifluoroacetyl)glycinate

: 1427753-07-8
tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)glycinate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane; water; ethyl acetate; hexane

2: potassium carbonate / water / 5 h / 20 °C

With potassium carbonate; triethylamine; In hexane; dichloromethane; water; ethyl acetate;

Reference yield:

: 943741-89-7
tert-butyl N-(3-nitrobenzyl)glycinate

: 1427753-07-8
tert-butyl N-(3-{[(tert-butoxycarbonyl)sulfamoyl]amino}benzyl)glycinate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 4 h / 20 °C / Cooling with ice

2: iron; ammonium chloride / water; ethanol / 1 h / 100 °C

3: triethylamine / dichloromethane; water; ethyl acetate; hexane

4: potassium carbonate / water / 5 h / 20 °C

With iron; potassium carbonate; ammonium chloride; triethylamine; In ethanol; hexane; dichloromethane; water; ethyl acetate;