(S)-2-{3-[3-(3-{3-[5-((S)-1,2-Dicarboxy-ethylcarbamoyl)-2-methyl-phenylcarbamoyl]-phenyl}-ureido)-benzoylamino]-4-methyl-benzoylamino}-succinic acid

Base Information

Chemical Name:(S)-2-{3-[3-(3-{3-[5-((S)-1,2-Dicarboxy-ethylcarbamoyl)-2-methyl-phenylcarbamoyl]-phenyl}-ureido)-benzoylamino]-4-methyl-benzoylamino}-succinic acid
CAS No.:133808-65-8
Molecular Formula:C₃₉H₃₆N₆O₁₃
Molecular Weight:796.747
Hs Code.:

Synonyms:(S)-2-{3-[3-(3-{3-[5-((S)-1,2-Dicarboxy-ethylcarbamoyl)-2-methyl-phenylcarbamoyl]-phenyl}-ureido)-benzoylamino]-4-methyl-benzoylamino}-succinic acid

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Chemical Property of (S)-2-{3-[3-(3-{3-[5-((S)-1,2-Dicarboxy-ethylcarbamoyl)-2-methyl-phenylcarbamoyl]-phenyl}-ureido)-benzoylamino]-4-methyl-benzoylamino}-succinic acid

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Technology Process of (S)-2-{3-[3-(3-{3-[5-((S)-1,2-Dicarboxy-ethylcarbamoyl)-2-methyl-phenylcarbamoyl]-phenyl}-ureido)-benzoylamino]-4-methyl-benzoylamino}-succinic acid

There total 5 articles about (S)-2-{3-[3-(3-{3-[5-((S)-1,2-Dicarboxy-ethylcarbamoyl)-2-methyl-phenylcarbamoyl]-phenyl}-ureido)-benzoylamino]-4-methyl-benzoylamino}-succinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 75-44-5
phosgene

: (S)-2-[3-(3-Amino-benzoylamino)-4-methyl-benzoylamino]-succinic acid

: 133808-65-8
(S)-2-{3-[3-(3-{3-[5-((S)-1,2-Dicarboxy-ethylcarbamoyl)-2-methyl-phenylcarbamoyl]-phenyl}-ureido)-benzoylamino]-4-methyl-benzoylamino}-succinic acid

Guidance literature:: With sodium hydroxide; In water; toluene;

Reference yield:

: 133808-47-6
N-(3-amino-4-methylbenzoyl)aspartic acid

: 133808-65-8
(S)-2-{3-[3-(3-{3-[5-((S)-1,2-Dicarboxy-ethylcarbamoyl)-2-methyl-phenylcarbamoyl]-phenyl}-ureido)-benzoylamino]-4-methyl-benzoylamino}-succinic acid

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH / H₂O; toluene / 4 h / Ambient temperature; pH 8

2: H₂ / 10percent Pd/C / H₂O; methanol / 4 h / Ambient temperature

3: 85 percent / NaOH / H₂O; toluene

With sodium hydroxide; hydrogen; palladium on activated charcoal; In methanol; water; toluene;

Reference yield:

: 133808-40-9
N-(4-methyl-3-nitrobenzyl)-L-aspartic acid

: 133808-65-8
(S)-2-{3-[3-(3-{3-[5-((S)-1,2-Dicarboxy-ethylcarbamoyl)-2-methyl-phenylcarbamoyl]-phenyl}-ureido)-benzoylamino]-4-methyl-benzoylamino}-succinic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / H₂ / 10percent Pd/C / H₂O; methanol / 4 h / Ambient temperature

2: NaOH / H₂O; toluene / 4 h / Ambient temperature; pH 8

3: H₂ / 10percent Pd/C / H₂O; methanol / 4 h / Ambient temperature

4: 85 percent / NaOH / H₂O; toluene

With sodium hydroxide; hydrogen; palladium on activated charcoal; In methanol; water; toluene;