6-diethoxyphosphorylmethyl-3,9-ditosyl-3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene

Base Information

• Chemical Name: 6-diethoxyphosphorylmethyl-3,9-ditosyl-3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene
• CAS No.: 308089-00-1
• Molecular Formula: C₃₀H₄₁N₄O₇PS₂
• Molecular Weight: 664.784

Synonyms:6-diethoxyphosphorylmethyl-3,9-ditosyl-3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene

Chemical Property of 6-diethoxyphosphorylmethyl-3,9-ditosyl-3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene

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Technology Process of 6-diethoxyphosphorylmethyl-3,9-ditosyl-3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene

There total 2 articles about 6-diethoxyphosphorylmethyl-3,9-ditosyl-3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2,6-bis(chloromethyl)pyridine (3099-28-3) + 4-diethoxyphosphorylmethyl-1,7-ditosyl-1,4,7-triazaheptane → 6-diethoxyphosphorylmethyl-3,9-ditosyl-3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(15),11,13-triene (308089-00-1)

Guidance literature:

With potassium carbonate; In acetonitrile; for 16h; Heating;

DOI:10.1021/jm000983a

Reference yield:

aminomethylphosphonic acid diethyl ester (50917-72-1) → 6-diethoxyphosphorylmethyl-3,9-ditosyl-3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(15),11,13-triene (308089-00-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / toluene / 6 h / Heating

2: 75 percent / K₂CO₃ / acetonitrile / 16 h / Heating

With potassium carbonate; In toluene; acetonitrile; 1: Ring cleavage / 2: Condensation;

DOI:10.1021/jm000983a

upstream raw materials:

2,6-bis(chloromethyl)pyridine

aminomethylphosphonic acid diethyl ester

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