4-nitro-2,2'-thiodibenzoic acid

Base Information

• Chemical Name: 4-nitro-2,2'-thiodibenzoic acid
• CAS No.: 103626-83-1
• Molecular Formula: C₁₄H₉NO₆S
• Molecular Weight: 319.295
• Mol file: 103626-83-1.mol

Synonyms:4-nitro-2,2'-thiodibenzoic acid

Chemical Property of 4-nitro-2,2'-thiodibenzoic acid

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-nitro-2,2'-thiodibenzoic acid

There total 1 articles about 4-nitro-2,2'-thiodibenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2-chloro-4-nitrobenzoic acid (99-60-5) + Thiosalicylic acid (147-93-3) → 4-nitro-2,2'-thiodibenzoic acid (103626-83-1)

Guidance literature:

Thiosalicylic acid; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃;

2-chloro-4-nitrobenzoic acid; With copper(I) oxide; for 5h; Reflux; Inert atmosphere;

DOI:10.1080/10426507.2012.685996

Reference yield: 81.0%

4-nitro-2,2'-thiodibenzoic acid (103626-83-1) + 2-amino-phenol (95-55-6) → N,N'-bis(2-hydroxyphenyl)-4-nitro-2,2'-thiodibenzamide (1393085-65-8)

Guidance literature:

4-nitro-2,2'-thiodibenzoic acid; With thionyl chloride; In dichloromethane; for 2h; Reflux;

2-amino-phenol;

DOI:10.1080/10426507.2012.685996

Reference yield: 76.0%

4-nitro-2,2'-thiodibenzoic acid (103626-83-1) + m-Hydroxyaniline (591-27-5) → N,N'-bis(3-hydroxyphenyl)-4-nitro-2,2'-thiodibenzamide (1393085-67-0)

Guidance literature:

4-nitro-2,2'-thiodibenzoic acid; With thionyl chloride; In dichloromethane; for 2h; Reflux;

m-Hydroxyaniline;

DOI:10.1080/10426507.2012.685996

upstream raw materials:

2-chloro-4-nitrobenzoic acid

Thiosalicylic acid

Downstream raw materials:

N,N'-dibenzyl-4-nitro-2,2'-thiodibenzamide

4-nitro-2,2'-thiodibenzanilide

N,N'-bis(2-methylphenyl)-4-nitro-2,2'-thiodibenzamide

N,N'-bis(2-hydroxyphenyl)-4-nitro-2,2'-thiodibenzamide