cyclohexylmethyl trifluoroacetate

Base Information

• Chemical Name: cyclohexylmethyl trifluoroacetate
• CAS No.: 164071-20-9
• Molecular Formula: C₉H₁₃F₃O₂
• Molecular Weight: 210.196
• Mol file: 164071-20-9.mol

Synonyms:cyclohexylmethyl trifluoroacetate

Chemical Property of cyclohexylmethyl trifluoroacetate

Chemical Property:

Purity/Quality:

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Technology Process of cyclohexylmethyl trifluoroacetate

There total 3 articles about cyclohexylmethyl trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

trifluoroacetic anhydride (407-25-0) + cyclohexylmethyl alcohol (100-49-2) → cyclohexylmethyl trifluoroacetate (164071-20-9)

Guidance literature:

In diethyl ether; at 0 ℃; for 1.33333h; Schlenk technique; Inert atmosphere; Glovebox;

DOI:10.1002/anie.201311221

Reference yield:

C10H13F3O4 → cyclohexylmethyl trifluoroacetate (164071-20-9) + cycloheptyl trifluoroacetate (777-58-2)

Guidance literature:

In trifluoroacetic acid; at -20 ℃; Product distribution;

DOI:10.1016/S0040-4039(02)02151-2

Reference yield:

→ cyclohexylmethyl trifluoroacetate (164071-20-9)

Guidance literature:

Cyclohexylmethanol, CF3COOOH, Na2HPO4;

DOI:10.1039/c39780000248

upstream raw materials:

trifluoroacetic anhydride

cyclohexylmethyl alcohol

Downstream raw materials:

2,2,2-trifluoroethanol

cyclohexylmethyl alcohol

Refernces

• 1、 Krasutsky, Pavel A.,Kolomitsyn, Igor V.,Botov, Evgenij M.,Carlson, Robert M.,Semenova, Irina G.,Fokin, Andrey A.. "Heterolytic decarboxylation involving acyltrifluoroacetyl peroxide intermediates". . p. 8687 - 8691. Retrieved 2007/10/03.