4-hydroxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

Base Information

Chemical Name:4-hydroxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether
CAS No.:270261-91-1
Molecular Formula:C₁₃H₁₈O₄
Molecular Weight:238.284
Hs Code.:

Synonyms:4-hydroxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

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Chemical Property of 4-hydroxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

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Technology Process of 4-hydroxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

There total 4 articles about 4-hydroxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 205381-75-5
4-benzyloxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

: 270261-91-1
4-hydroxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 4h; under 2250.23 Torr; Inert atmosphere;
DOI:10.1002/cmdc.201500100

Reference yield: 60.0%

: C₁₈H₂₆O₅

: 270261-91-1
4-hydroxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

Guidance literature:: With aluminium(III) iodide; N,N-dimethyl-formamide dimethyl acetal; In acetonitrile; at 20 ℃; for 0.5h;
DOI:10.1021/acs.joc.0c00290

Reference yield:

: 103-16-2
4-Benzyloxyphenol

: 270261-91-1
4-hydroxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 20 °C / Inert atmosphere

1.2: 0.08 h / Inert atmosphere

2.1: 5%-palladium/activated carbon; hydrogen / ethyl acetate / 4 h / 20 °C / 2250.23 Torr / Inert atmosphere

With 5%-palladium/activated carbon; hydrogen; potassium hydroxide; In dimethyl sulfoxide; ethyl acetate;
DOI:10.1002/cmdc.201500100