3,4-dimethoxyphenyl 3-hydroxy-3-(3,4-methylenedioxyphenyl)propyl ketone

Base Information

• Chemical Name: 3,4-dimethoxyphenyl 3-hydroxy-3-(3,4-methylenedioxyphenyl)propyl ketone
• CAS No.: 76934-69-5
• Molecular Formula: C₁₉H₂₀O₆
• Molecular Weight: 344.364
• Mol file: 76934-69-5.mol

Synonyms:3,4-dimethoxyphenyl 3-hydroxy-3-(3,4-methylenedioxyphenyl)propyl ketone

Chemical Property of 3,4-dimethoxyphenyl 3-hydroxy-3-(3,4-methylenedioxyphenyl)propyl ketone

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 3,4-dimethoxyphenyl 3-hydroxy-3-(3,4-methylenedioxyphenyl)propyl ketone

There total 2 articles about 3,4-dimethoxyphenyl 3-hydroxy-3-(3,4-methylenedioxyphenyl)propyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

(2-Benzo[1,3]dioxol-5-yl-cyclopropyl)-(3,4-dimethoxy-phenyl)-methanone (76934-56-0) → 6,7-dimethoxy-4-(3,4-methylenedioxyphenyl)-3,4-dihydronaphthalen-1(2H)-one (80816-89-3) + 3,4-dimethoxyphenyl 3-hydroxy-3-(3,4-methylenedioxyphenyl)propyl ketone (76934-69-5)

Guidance literature:

With tin(IV) chloride; In nitromethane; for 30h; Ambient temperature;

DOI:10.1039/P19810002920

Reference yield: 35.0%

((1S,2S)-2-Benzo[1,3]dioxol-5-yl-cyclopropyl)-(3,4-dimethoxy-phenyl)-methanone (76934-56-0) → 6,7-dimethoxy-4-(3,4-methylenedioxyphenyl)-3,4-dihydronaphthalen-1(2H)-one (80816-89-3) + 3,4-dimethoxyphenyl 3-hydroxy-3-(3,4-methylenedioxyphenyl)propyl ketone (76934-69-5)

Guidance literature:

With tin(IV) chloride; In benzene; for 47h; Ambient temperature;

upstream raw materials:

(2-Benzo[1,3]dioxol-5-yl-cyclopropyl)-(3,4-dimethoxy-phenyl)-methanone

((1S,2S)-2-Benzo[1,3]dioxol-5-yl-cyclopropyl)-(3,4-dimethoxy-phenyl)-methanone