(R)-2-(4-fluoro-3,5-dimethylphenylamino)hexanoic acid tert-butoxyamide

Base Information

Chemical Name:(R)-2-(4-fluoro-3,5-dimethylphenylamino)hexanoic acid tert-butoxyamide
CAS No.:1043890-86-3
Molecular Formula:C₁₈H₂₉FN₂O₂
Molecular Weight:324.439
Hs Code.:

Synonyms:(R)-2-(4-fluoro-3,5-dimethylphenylamino)hexanoic acid tert-butoxyamide

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Chemical Property of (R)-2-(4-fluoro-3,5-dimethylphenylamino)hexanoic acid tert-butoxyamide

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Technology Process of (R)-2-(4-fluoro-3,5-dimethylphenylamino)hexanoic acid tert-butoxyamide

There total 3 articles about (R)-2-(4-fluoro-3,5-dimethylphenylamino)hexanoic acid tert-butoxyamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 37477-16-0
O-(tert-butyl)hydroxylamine

: 1043890-85-2
(R)-2-(4-fluoro-3,5-dimethylphenylamino)hexanoic acid

: 1043890-86-3
(R)-2-(4-fluoro-3,5-dimethylphenylamino)hexanoic acid tert-butoxyamide

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 44h;

Reference yield:

: 327-56-0
D-norleucine

: 1043890-86-3
(R)-2-(4-fluoro-3,5-dimethylphenylamino)hexanoic acid tert-butoxyamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(l) iodide; potassium carbonate / ISOPROPYLAMIDE / 39 h / 90 °C

1.2: 20 °C / pH 3

2.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 44 h / 20 °C

With 4-methyl-morpholine; copper(l) iodide; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; ISOPROPYLAMIDE;

Reference yield:

: 99725-44-7
3,5-dimethyl-4-fluoro-1-bromobenzene

: 1043890-86-3
(R)-2-(4-fluoro-3,5-dimethylphenylamino)hexanoic acid tert-butoxyamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(l) iodide; potassium carbonate / ISOPROPYLAMIDE / 39 h / 90 °C

1.2: 20 °C / pH 3

2.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 44 h / 20 °C

With 4-methyl-morpholine; copper(l) iodide; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; ISOPROPYLAMIDE;