methyl 3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idoheptofuranuronate

Base Information

Chemical Name:methyl 3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idoheptofuranuronate
CAS No.:1318961-01-1
Molecular Formula:C₃₁H₃₅NO₆
Molecular Weight:517.622
Hs Code.:

Synonyms:methyl 3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idoheptofuranuronate

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Chemical Property of methyl 3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idoheptofuranuronate

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Technology Process of methyl 3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idoheptofuranuronate

There total 1 articles about methyl 3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idoheptofuranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 591727-19-4
1-2,5-6 di-O-isopropylidene 3-O-benzyl α(D)gluco-pentoaldofuranose

: 1318961-01-1
methyl 3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idoheptofuranuronate

: 1318961-39-5
C₃₁H₃₅NO₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; acetic acid / 24 h

1.2: 2 h

1.3: 1 h / 0 °C

2.1: methanol / tetrahydrofuran / 24 h / 25 °C / 9000900 Torr

With methanol; water; acetic acid; In tetrahydrofuran; 1.3: Wittig reaction / 2.1: aza-Michael addition;
DOI:10.1039/c1gc15097a

Reference yield: 64.0%

: 1318961-01-1
methyl 3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idoheptofuranuronate

: 1318961-08-8
3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idohepto-1,4-furanose

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c1gc15097a

Reference yield:

: 1318961-01-1
methyl 3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idoheptofuranuronate

: C₁₄H₂₁NO₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

2.1: water; trifluoroacetic acid / 1.5 h / 40 °C

2.2: 12 h / 4500.45 Torr

With lithium aluminium tetrahydride; water; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1039/c1gc15097a