3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idohepto-1,4-furanose

Base Information

Chemical Name:3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idohepto-1,4-furanose
CAS No.:1318961-08-8
Molecular Formula:C₃₀H₃₅NO₅
Molecular Weight:489.612
Hs Code.:

Synonyms:3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idohepto-1,4-furanose

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Chemical Property of 3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idohepto-1,4-furanose

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Technology Process of 3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idohepto-1,4-furanose

There total 4 articles about 3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idohepto-1,4-furanose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1318961-01-1
methyl 3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idoheptofuranuronate

: 1318961-08-8
3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idohepto-1,4-furanose

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c1gc15097a

Reference yield:

: 591727-19-4
1-2,5-6 di-O-isopropylidene 3-O-benzyl α(D)gluco-pentoaldofuranose

: 1318961-08-8
3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idohepto-1,4-furanose

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; acetic acid / 24 h

1.2: 2 h

1.3: 1 h / 0 °C

2.1: methanol / tetrahydrofuran / 24 h / 25 °C / 9000900 Torr

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

With methanol; lithium aluminium tetrahydride; water; acetic acid; In tetrahydrofuran; 1.3: Wittig reaction / 2.1: aza-Michael addition;
DOI:10.1039/c1gc15097a

Reference yield:

: 77399-49-6
methyl (E)-3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hept-5-enofuranuronate

: 1318961-08-8
3-O-benzyl-5-(N-diphenylmethylamino)-5,6-dideoxy-1,2-O-isopropylidene-β-L-idohepto-1,4-furanose

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / tetrahydrofuran / 24 h / 25 °C / 9000900 Torr

2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

With methanol; lithium aluminium tetrahydride; In tetrahydrofuran; 1: aza-Michael addition;
DOI:10.1039/c1gc15097a