1-[(4-benzyl)-5-(3-pyridyl)-4H-1,2,4-triazol-3-ylthiomethylcarboxyl]-3,5-dimethyl-1H-pyrazole

Base Information

Chemical Name:1-[(4-benzyl)-5-(3-pyridyl)-4H-1,2,4-triazol-3-ylthiomethylcarboxyl]-3,5-dimethyl-1H-pyrazole
CAS No.:1352049-57-0
Molecular Formula:C₂₁H₂₀N₆OS
Molecular Weight:404.495
Hs Code.:

Synonyms:1-[(4-benzyl)-5-(3-pyridyl)-4H-1,2,4-triazol-3-ylthiomethylcarboxyl]-3,5-dimethyl-1H-pyrazole

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Chemical Property of 1-[(4-benzyl)-5-(3-pyridyl)-4H-1,2,4-triazol-3-ylthiomethylcarboxyl]-3,5-dimethyl-1H-pyrazole

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Technology Process of 1-[(4-benzyl)-5-(3-pyridyl)-4H-1,2,4-triazol-3-ylthiomethylcarboxyl]-3,5-dimethyl-1H-pyrazole

There total 4 articles about 1-[(4-benzyl)-5-(3-pyridyl)-4H-1,2,4-triazol-3-ylthiomethylcarboxyl]-3,5-dimethyl-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1352049-52-5
2-[-4-benzyl-5-(3-pyridyl)-4H-1,2,4-triazole-3-ylthio]-N⁽²⁾-[1-methyl-3-oxobutilidin]acetohydrazine

: 1352049-57-0
1-[(4-benzyl)-5-(3-pyridyl)-4H-1,2,4-triazol-3-ylthiomethylcarboxyl]-3,5-dimethyl-1H-pyrazole

Guidance literature:: With hydrogenchloride; In ethanol; water; for 30h; Reflux;
DOI:10.1002/jhet.718

Reference yield:

: 359010-76-7
C₁₆H₁₆N₆OS

: 1352049-57-0
1-[(4-benzyl)-5-(3-pyridyl)-4H-1,2,4-triazol-3-ylthiomethylcarboxyl]-3,5-dimethyl-1H-pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 5 h / Reflux

2: hydrogenchloride / ethanol; water / 30 h / Reflux

With hydrogenchloride; In ethanol; water;
DOI:10.1002/jhet.718

Reference yield:

: 129119-80-8
4-benzyl-5-(pyridin-3-yl)-4H-1,2,4-triazole-3-thiol

: 1352049-57-0
1-[(4-benzyl)-5-(3-pyridyl)-4H-1,2,4-triazol-3-ylthiomethylcarboxyl]-3,5-dimethyl-1H-pyrazole

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / ethanol / Reflux

2: hydrazine hydrate / ethanol / Reflux

3: ethanol / 5 h / Reflux

4: hydrogenchloride / ethanol; water / 30 h / Reflux

With hydrogenchloride; hydrazine hydrate; sodium hydroxide; In ethanol; water;
DOI:10.1002/jhet.718