2-benzyloxy-4-phenylacetophenone

Base Information

Chemical Name:2-benzyloxy-4-phenylacetophenone
CAS No.:1338384-39-6
Molecular Formula:C₂₁H₁₈O₂
Molecular Weight:302.373
Hs Code.:

Synonyms:2-benzyloxy-4-phenylacetophenone

Suppliers and Price of 2-benzyloxy-4-phenylacetophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-benzyloxy-4-phenylacetophenone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-benzyloxy-4-phenylacetophenone

There total 1 articles about 2-benzyloxy-4-phenylacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 32101-38-5
2-hydroxy-4-phenyl-acetophenone

: 100-39-0
benzyl bromide

: 1338384-39-6
2-benzyloxy-4-phenylacetophenone

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; Reflux;
DOI:10.1021/jm200937t

Reference yield: 78.0%

: 1338384-39-6
2-benzyloxy-4-phenylacetophenone

: 1338384-42-1
2-benzyloxy-4-phenylphenol

Guidance literature:: 2-benzyloxy-4-phenylacetophenone; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 48h;

With sodium hydroxide; In methanol; for 2h;

With hydrogenchloride; In methanol; water;
DOI:10.1021/jm200937t

Reference yield:

: 1338384-39-6
2-benzyloxy-4-phenylacetophenone

: 1338384-76-1
(1R,2'S)-1-(1'-Boc-2'-pyrrolidinyl)-2-(o-hydroxy-p-phenylphenoxy)ethanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 48 h / 0 - 20 °C

1.2: 2 h

2.1: sodium hydroxide / methanol

2.2: 20 °C

3.1: sodium tetrahydroborate / tetrahydrofuran / -20 - -10 °C

4.1: palladium 10% on activated carbon; hydrogen / methanol / 48 h / 20 °C / 760.05 Torr

With sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; 1.1: Dakin reaction / 1.2: Dakin reaction;
DOI:10.1021/jm200937t