CBzGly-Aib₄-OH

Base Information

Chemical Name:CBzGly-Aib₄-OH
CAS No.:1187839-13-9
Molecular Formula:C₂₆H₃₉N₅O₈
Molecular Weight:549.624
Hs Code.:

Synonyms:CBzGly-Aib₄-OH

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Chemical Property of CBzGly-Aib₄-OH

Chemical Property:

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Technology Process of CBzGly-Aib₄-OH

There total 4 articles about CBzGly-Aib₄-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: Z-Gly-(Aib)₄-N(Me)Ph

: 1187839-13-9
CBzGly-Aib₄-OH

Guidance literature:: With hydrogenchloride; water; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1002/hlca.201400359

Reference yield: 92.0%

: 1187839-08-2
CBzGly-Aib₄-O^tBu

: 1187839-13-9
CBzGly-Aib₄-OH

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/anie.200901892

Reference yield:

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 1187839-13-9
CBzGly-Aib₄-OH

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; O-Benzotriazol-1-yl-N,N,N',N'-bis(tetramethylene)uronium hexafluorophosphate / dichloromethane / 21 h / 20 °C

2: hydrogenchloride; water / tetrahydrofuran / 1 h / 20 °C

With hydrogenchloride; water; O-Benzotriazol-1-yl-N,N,N',N'-bis(tetramethylene)uronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/hlca.201400359