1-(cyclohex-1-en-1-yloxy)-N,N-diethyl-1,1-dimethylsilanamine

Base Information

• Chemical Name: 1-(cyclohex-1-en-1-yloxy)-N,N-diethyl-1,1-dimethylsilanamine
• CAS No.: 1638623-22-9
• Molecular Formula: C₁₂H₂₅NOSi
• Molecular Weight: 227.422
• Mol file: 1638623-22-9.mol

Synonyms:1-(cyclohex-1-en-1-yloxy)-N,N-diethyl-1,1-dimethylsilanamine

Chemical Property of 1-(cyclohex-1-en-1-yloxy)-N,N-diethyl-1,1-dimethylsilanamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(cyclohex-1-en-1-yloxy)-N,N-diethyl-1,1-dimethylsilanamine

There total 1 articles about 1-(cyclohex-1-en-1-yloxy)-N,N-diethyl-1,1-dimethylsilanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(N,N-diethylamino)dimethylchlorosilane (6026-02-4) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → 1-(cyclohex-1-en-1-yloxy)-N,N-diethyl-1,1-dimethylsilanamine (1638623-22-9)

Guidance literature:

(N,N-diethylamino)dimethylchlorosilane; With sodium iodide; In acetonitrile; at 25 ℃; for 0.166667h; Inert atmosphere; Schlenk technique;

cyclohexanone; With triethylamine; In acetonitrile; at 25 ℃; for 2h; Inert atmosphere; Schlenk technique;

DOI:10.1002/anie.201400405

Reference yield: 87.0%

1-(cyclohex-1-en-1-yloxy)-N,N-diethyl-1,1-dimethylsilanamine (1638623-22-9) → 2-(diethylamino)cyclohexanone (52061-84-4)

Guidance literature:

With [bis(acetoxy)iodo]benzene; In dichloromethane; at 25 ℃; Inert atmosphere; Schlenk technique;

DOI:10.1002/anie.201400405

Reference yield:

1-(cyclohex-1-en-1-yloxy)-N,N-diethyl-1,1-dimethylsilanamine (1638623-22-9) → C8H15ClOSi (58101-72-7)

Guidance literature:

With acetyl chloride; In tetrahydrofuran; at 0 ℃; for 0.333333h; Inert atmosphere; Schlenk technique;

DOI:10.1002/anie.201400405

upstream raw materials:

(N,N-diethylamino)dimethylchlorosilane

cyclohexanone

Downstream raw materials:

(cyclohex-1-en-1-yloxy)(ethoxy)dimethylsilane

(cyclohex-1-en-1-yloxy)dimethylsilyl acetate

2-(diethylamino)cyclohexanone

(R)-2-(diethylamino)cyclohexanone