benzyl 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-bromoethyl phosphate

Base Information

Chemical Name:benzyl 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-bromoethyl phosphate
CAS No.:1323910-16-2
Molecular Formula:C₅₈H₉₆BrN₂O₄P
Molecular Weight:996.289
Hs Code.:

Synonyms:benzyl 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-bromoethyl phosphate

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Chemical Property of benzyl 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-bromoethyl phosphate

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Technology Process of benzyl 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-bromoethyl phosphate

There total 9 articles about benzyl 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-bromoethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₈H₉₆BrN₂O₃P

: 1323910-16-2
benzyl 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-bromoethyl phosphate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.06.031

Reference yield:

: 143-27-1
hexadecylamine

: 1323910-16-2
benzyl 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-bromoethyl phosphate

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 80 °C / Inert atmosphere

2.2: 0.25 h / 0 °C

3.1: ethanol / 1 h / 150 °C / Microwave irradiation

4.1: triethylamine / tetrahydrofuran / 20 h / 0 °C / Inert atmosphere

5.1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

6.1: 3-chloro-benzenecarboperoxoic acid / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.tetlet.2011.06.031

Reference yield:

: C₅₆H₉₂ClN₂O₂P

: 1323910-16-2
benzyl 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-bromoethyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2011.06.031