Technology Process of benzyl 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-bromoethyl phosphate
There total 9 articles about benzyl 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-bromoethyl phosphate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1016/j.tetlet.2011.06.031
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 80 °C / Inert atmosphere
2.2: 0.25 h / 0 °C
3.1: ethanol / 1 h / 150 °C / Microwave irradiation
4.1: triethylamine / tetrahydrofuran / 20 h / 0 °C / Inert atmosphere
5.1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
6.1: 3-chloro-benzenecarboperoxoic acid / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.tetlet.2011.06.031
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
With
triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran;
DOI:10.1016/j.tetlet.2011.06.031
