1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-(trimethylammonio)ethyl phosphate

Base Information

Chemical Name:1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-(trimethylammonio)ethyl phosphate
CAS No.:1323910-17-3
Molecular Formula:C₅₄H₉₈N₃O₄P
Molecular Weight:884.364
Hs Code.:

Synonyms:1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-(trimethylammonio)ethyl phosphate

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Chemical Property of 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-(trimethylammonio)ethyl phosphate

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Technology Process of 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-(trimethylammonio)ethyl phosphate

There total 8 articles about 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-(trimethylammonio)ethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1323910-16-2
benzyl 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-bromoethyl phosphate

: 75-50-3
trimethylamine

: 1323910-17-3
1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-(trimethylammonio)ethyl phosphate

Guidance literature:: benzyl 1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-bromoethyl phosphate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

trimethylamine; In chloroform; isopropyl alcohol; acetonitrile; for 24h;
DOI:10.1016/j.tetlet.2011.06.031

Reference yield:

: 143-27-1
hexadecylamine

: 1323910-17-3
1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-(trimethylammonio)ethyl phosphate

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 80 °C / Inert atmosphere

2.2: 0.25 h / 0 °C

3.1: ethanol / 1 h / 150 °C / Microwave irradiation

4.1: triethylamine / tetrahydrofuran / 20 h / 0 °C / Inert atmosphere

5.1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

6.1: 3-chloro-benzenecarboperoxoic acid / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

7.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

7.2: 24 h

With lithium aluminium tetrahydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.tetlet.2011.06.031

Reference yield:

: C₅₆H₉₂ClN₂O₂P

: 1323910-17-3
1,3-bis(benzyl(hexadecyl)amino)propan-2-yl 2-(trimethylammonio)ethyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

3.2: 24 h

With triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2011.06.031