4-deuterated benzaldehyde

Base Information

• Chemical Name: 4-deuterated benzaldehyde
• CAS No.: 33836-85-0
• Molecular Formula: C₇H₆O
• Molecular Weight: 107.116
• Mol file: 33836-85-0.mol

Synonyms:4-deuterated benzaldehyde

Chemical Property of 4-deuterated benzaldehyde

Chemical Property:

Purity/Quality:

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Technology Process of 4-deuterated benzaldehyde

There total 15 articles about 4-deuterated benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

4-bromo-benzaldehyde (1122-91-4) → 4-deuterated benzaldehyde (33836-85-0)

Guidance literature:

With sodium formate; dimethyl sulfoxide; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; at 80 ℃; for 8h; Inert atmosphere;

Reference yield: 75.0%

2-(4-deuteriophenyl)-1,3-dioxolane → 4-deuterated benzaldehyde (33836-85-0)

Guidance literature:

With toluene-4-sulfonic acid; acetone; at 20 ℃;

DOI:10.1002/ejoc.200701224

Reference yield: 8.0%

4-deuteriotoluene (4409-83-0) → p-cresol (106-44-5) + 4-deuterated benzaldehyde (33836-85-0) + 4-deuterobenzyl alcohol (13122-27-5) + 3-methyl-phenol (108-39-4) + C7H7(2)HO (116467-72-2) + C7H7(2)HO (116467-71-1)

Guidance literature:

With ferrous perchlorate; copper(II) ion; dihydrogen peroxide; In water; acetonitrile; at 25 ℃; for 0.5h; Mechanism; Product distribution; further oxidants and solvents;

DOI:10.1021/ja00230a032

upstream raw materials:

methanol

4-deuteriotoluene

[4-²H]benzyl bromide

para-bromotoluene

Downstream raw materials:

trans-4,4'-dideuterio-stilbene

4-deuteriohydrocinnamic acid

4-deuteriocinnamic acid