1',2',3',4',5'-penta-O-acetyl-1'-C-[(4R,5R)-1,2-dimethyl-4-nitrocyclohex-1-en-5-yl]-D-manno-pentitol

Base Information

• Chemical Name: 1',2',3',4',5'-penta-O-acetyl-1'-C-[(4R,5R)-1,2-dimethyl-4-nitrocyclohex-1-en-5-yl]-D-manno-pentitol
• CAS No.: 438625-50-4
• Molecular Formula: C₂₃H₃₃NO₁₂
• Molecular Weight: 515.515

Synonyms:1',2',3',4',5'-penta-O-acetyl-1'-C-[(4R,5R)-1,2-dimethyl-4-nitrocyclohex-1-en-5-yl]-D-manno-pentitol

Chemical Property of 1',2',3',4',5'-penta-O-acetyl-1'-C-[(4R,5R)-1,2-dimethyl-4-nitrocyclohex-1-en-5-yl]-D-manno-pentitol

Chemical Property:

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Technology Process of 1',2',3',4',5'-penta-O-acetyl-1'-C-[(4R,5R)-1,2-dimethyl-4-nitrocyclohex-1-en-5-yl]-D-manno-pentitol

There total 1 articles about 1',2',3',4',5'-penta-O-acetyl-1'-C-[(4R,5R)-1,2-dimethyl-4-nitrocyclohex-1-en-5-yl]-D-manno-pentitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

(E)-3,4,5,6,7-penta-O-acetyl-1,2-dideoxy-1-C-nitro-D-manno-hept-1-enitol (119479-73-1) + 2,3-dimethyl-buta-1,3-diene (513-81-5) → 1',2',3',4',5'-penta-O-acetyl-1'-C-[(4R,5R)-1,2-dimethyl-4-nitrocyclohex-1-en-5-yl]-D-manno-pentitol (438625-50-4) + (4S,5S)-1,2,3,4,5-penta-O-acetyl-1-C-(1,2-dimethyl-4-nitrocyclohex-1-en-5-yl)-D-manno-pentitol (955378-01-5)

Guidance literature:

In toluene; at 105 ℃;

Reference yield: 100.0%

1',2',3',4',5'-penta-O-acetyl-1'-C-[(4R,5R)-1,2-dimethyl-4-nitrocyclohex-1-en-5-yl]-D-manno-pentitol (438625-50-4) → (4R,5R)-1-C-(1,2-dimethyl-4-nitrocyclohex-1-en-5-yl)-D-manno-pentitol (125488-62-2)

Guidance literature:

With hydrogenchloride; In methanol; for 4h; Heating;

DOI:10.1016/S0040-4020(02)00487-8

Reference yield: 89.0%

1',2',3',4',5'-penta-O-acetyl-1'-C-[(4R,5R)-1,2-dimethyl-4-nitrocyclohex-1-en-5-yl]-D-manno-pentitol (438625-50-4) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → 1',2',3',4',5'-penta-O-acetyl-1'-C-[(4S,5R)-1,2-dimethyl-4-(2''-methoxycarbonylethyl)-4-nitrocyclohex-1-en-5-yl]-D-manno-pentitol (217298-50-5)

Guidance literature:

With N,N,N',N'-tetramethylguanidine; In acetonitrile; Ambient temperature;

DOI:10.1016/S0040-4039(98)01911-X

upstream raw materials:

(E)-3,4,5,6,7-penta-O-acetyl-1,2-dideoxy-1-C-nitro-D-manno-hept-1-enitol

2,3-dimethyl-buta-1,3-diene

Downstream raw materials:

4,5-dimethylcyclohexa-1,4-diene-1-carbaldehyde

(4R,5R)-1-C-(1,2-dimethyl-4-nitrocyclohex-1-en-5-yl)carbaldehyde

(1R,2R,3R,4R)-1-((R)-3,4-Dimethyl-6-nitro-cyclohex-3-enyl)-pentane-1,2,3,4,5-pentaol

(4S,5R)-1-C-(1,2-dimethyl-4-nitrocyclohex-1-en-5-yl)-D-manno-pentitol

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