6--O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serylamino>capronsaeure-methylester

Base Information

Chemical Name:6--O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serylamino>capronsaeure-methylester
CAS No.:107222-76-4
Molecular Formula:C₅₈H₇₃N₃O₂₄
Molecular Weight:1196.22
Hs Code.:

6-<N-<2-Acetamido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyloxycarbonyl>-O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serylamino>capronsaeure-methylester

Synonyms:6--O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serylamino>capronsaeure-methylester

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Chemical Property of 6--O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serylamino>capronsaeure-methylester

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Technology Process of 6--O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serylamino>capronsaeure-methylester

There total 6 articles about 6--O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serylamino>capronsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107222-69-5
N-(3,5-Dimethoxy-α,α-dimethylbenzyloxycarbonyl)-L-serin-benzylester

: 107222-76-4
6--O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serylamino>capronsaeure-methylester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) molecular sieve (4 Angstroem), drierite, Ag₂CO₃; 2.) AgClO₄ / 1.) CH₂Cl₂, toluene, 0 deg C, 0.5 h; CH₂Cl₂, toluene, 20 h

2: 93 percent / hydrogen / Pd/C (10percent Pd) / ethyl acetate / 2 h

4: 1.) H₂, conc. ammonia / 1.) Pd/C (10percent Pd) / 1.) methanol, 4 h; 2.) methanol, 4 deg C, 12 h

With calcium sulfate; ammonium hydroxide; 4 A molecular sieve; hydrogen; silver perchlorate; silver carbonate; 10% palladium on active carbon; In ethyl acetate;

Reference yield:

: 96043-05-9
2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-galactopyranosylchlorid

: 107222-76-4
6--O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serylamino>capronsaeure-methylester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) molecular sieve (4 Angstroem), drierite, Ag₂CO₃; 2.) AgClO₄ / 1.) CH₂Cl₂, toluene, 0 deg C, 0.5 h; CH₂Cl₂, toluene, 20 h

2: 93 percent / hydrogen / Pd/C (10percent Pd) / ethyl acetate / 2 h

4: 1.) H₂, conc. ammonia / 1.) Pd/C (10percent Pd) / 1.) methanol, 4 h; 2.) methanol, 4 deg C, 12 h

With calcium sulfate; ammonium hydroxide; 4 A molecular sieve; hydrogen; silver perchlorate; silver carbonate; 10% palladium on active carbon; In ethyl acetate;

Reference yield:

: N-<2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyloxycarbonyl>-O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serin-benzylester

: 107222-76-4
6--O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serylamino>capronsaeure-methylester

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / hydrogen / Pd/C (10percent Pd) / ethyl acetate / 2 h

3: 1.) H₂, conc. ammonia / 1.) Pd/C (10percent Pd) / 1.) methanol, 4 h; 2.) methanol, 4 deg C, 12 h

With ammonium hydroxide; hydrogen; 10% palladium on active carbon; In ethyl acetate;