5-dibenzyl L-1,2-O-cyclohexylidene-6-O-levulinoyl-myo-inositol phosphate

Base Information

Chemical Name:5-dibenzyl L-1,2-O-cyclohexylidene-6-O-levulinoyl-myo-inositol phosphate
CAS No.:608880-25-7
Molecular Formula:C₃₁H₃₉O₁₁P
Molecular Weight:618.618
Hs Code.:

Synonyms:5-dibenzyl L-1,2-O-cyclohexylidene-6-O-levulinoyl-myo-inositol phosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-dibenzyl L-1,2-O-cyclohexylidene-6-O-levulinoyl-myo-inositol phosphate

Chemical Property:

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Technology Process of 5-dibenzyl L-1,2-O-cyclohexylidene-6-O-levulinoyl-myo-inositol phosphate

There total 5 articles about 5-dibenzyl L-1,2-O-cyclohexylidene-6-O-levulinoyl-myo-inositol phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 608880-23-5
5-dibenzyl L-1,2-O-cyclohexylidene-6-O-levulinoyl-3,4-O-(tetraisopropyldisiloxane-1,3-diyl)-myo-inositol phosphate

: 608880-25-7
5-dibenzyl L-1,2-O-cyclohexylidene-6-O-levulinoyl-myo-inositol phosphate

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at -15 - -10 ℃; for 4.5h;
DOI:10.1002/ejoc.200300517

Reference yield:

: 123-76-2
levulinic acid

: 608880-25-7
5-dibenzyl L-1,2-O-cyclohexylidene-6-O-levulinoyl-myo-inositol phosphate

Guidance literature:: Multi-step reaction with 3 steps

1.1: DCC; DMAP / CH₂Cl₂ / 20 °C

2.1: 1H-tetrazole / CH₂Cl₂ / 1 h / 20 °C

2.2: 95 percent / water; mCPBA / CH₂Cl₂ / 1 h / 20 °C

3.1: 88 percent / AcOH; TBAF*3H₂O / tetrahydrofuran / 4.5 h / -15 - -10 °C

With 1H-tetrazole; dmap; tetrabutyl ammonium fluoride; acetic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.200300517

Reference yield:

: 247088-70-6
L-1,2-O-cyclohexylidene-3,4-O-(tetraisopropyl-disiloxane-1,3-diyl)-6-O-[(S)-O-acetylmandeloyl]-myo-inositol

: 608880-25-7
5-dibenzyl L-1,2-O-cyclohexylidene-6-O-levulinoyl-myo-inositol phosphate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 100 percent / hydrazine hydrate / dimethylformamide / 1.5 h / 20 °C

2.1: DCC; DMAP / CH₂Cl₂ / 20 °C

3.1: 1H-tetrazole / CH₂Cl₂ / 1 h / 20 °C

3.2: 95 percent / water; mCPBA / CH₂Cl₂ / 1 h / 20 °C

4.1: 88 percent / AcOH; TBAF*3H₂O / tetrahydrofuran / 4.5 h / -15 - -10 °C

With 1H-tetrazole; dmap; tetrabutyl ammonium fluoride; hydrazine hydrate; acetic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200300517