benzyl cyclohexyl methyl phosphate

Base Information

• Chemical Name: benzyl cyclohexyl methyl phosphate
• CAS No.: 173170-94-0
• Molecular Formula: C₁₄H₂₁O₄P
• Molecular Weight: 284.292
• Mol file: 173170-94-0.mol

Synonyms:benzyl cyclohexyl methyl phosphate

Chemical Property of benzyl cyclohexyl methyl phosphate

Chemical Property:

Purity/Quality:

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Technology Process of benzyl cyclohexyl methyl phosphate

There total 2 articles about benzyl cyclohexyl methyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Phosphorous acid benzyl ester cyclohexyl ester methyl ester → benzyl cyclohexyl methyl phosphate (173170-94-0)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 1h; Yield given;

DOI:10.1021/ja00154a017

Reference yield:

benzyl methyl N,N-diisopropylphosphoramidite (173170-93-9) → benzyl cyclohexyl methyl phosphate (173170-94-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1H-tetrazole / CH₂Cl₂ / 2 h

2: 85percent 3-chloroperoxybenzoic acid / CH₂Cl₂ / 1 h

With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1021/ja00154a017

Reference yield: 98.0%

benzyl cyclohexyl methyl phosphate (173170-94-0) → benzyl cyclohexyl phosphate (51174-13-1)

Guidance literature:

With lithium cyanide; In N,N-dimethyl-formamide; for 20h;

DOI:10.1021/ja00154a017

upstream raw materials:

benzyl methyl N,N-diisopropylphosphoramidite

Downstream raw materials:

benzyl cyclohexyl phosphate

cyclohexyl tribenzyl pyrophosphate