Thexyldimethylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-β-D-xylo-4-hexulopyranoside

Base Information

Chemical Name:Thexyldimethylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-β-D-xylo-4-hexulopyranoside
CAS No.:174077-03-3
Molecular Formula:C₂₈H₃₉N₃O₅Si
Molecular Weight:525.72
Hs Code.:

Synonyms:Thexyldimethylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-β-D-xylo-4-hexulopyranoside

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Chemical Property of Thexyldimethylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-β-D-xylo-4-hexulopyranoside

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Technology Process of Thexyldimethylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-β-D-xylo-4-hexulopyranoside

There total 5 articles about Thexyldimethylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-β-D-xylo-4-hexulopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 174077-02-2
dimethylthexylsilyl 3,6-di-O-benzyl-2-deoxy-2-azido-β-D-glucopyranoside

: 174077-03-3
Thexyldimethylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-β-D-xylo-4-hexulopyranoside

Guidance literature:: With Dess-Martin periodane; In dichloromethane; for 1h; Ambient temperature;

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 174077-03-3
Thexyldimethylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-β-D-xylo-4-hexulopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / p-TsOH / acetonitrile / 1 h

2: 93 percent / NaH / dimethylformamide / 2 h / -15 °C

3: 86 percent / NaCNBH₃, HCl / diethyl ether; tetrahydrofuran

4: 95 percent / 1,1,1-triacetoxy-1,1-dihydro-1,2-benzodioxol-3(1H)-one / CH₂Cl₂ / 1 h / Ambient temperature

With hydrogenchloride; sodium hydride; sodium cyanoborohydride; Dess-Martin periodane; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 157488-88-5
thexyldimethylsilyl 2-azido-2-deoxy-β-D-glucopyranoside

: 174077-03-3
Thexyldimethylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-β-D-xylo-4-hexulopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / p-TsOH / acetonitrile / 1 h

2: 93 percent / NaH / dimethylformamide / 2 h / -15 °C

3: 86 percent / NaCNBH₃, HCl / diethyl ether; tetrahydrofuran

4: 95 percent / 1,1,1-triacetoxy-1,1-dihydro-1,2-benzodioxol-3(1H)-one / CH₂Cl₂ / 1 h / Ambient temperature

With hydrogenchloride; sodium hydride; sodium cyanoborohydride; Dess-Martin periodane; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;