C₁₃H₁₇NO₂S

Base Information

• Chemical Name: C₁₃H₁₇NO₂S
• CAS No.: 1611453-98-5
• Molecular Formula: C₁₃H₁₇NO₂S
• Molecular Weight: 251.349
• Mol file: 1611453-98-5.mol

Synonyms:C₁₃H₁₇NO₂S

Chemical Property of C₁₃H₁₇NO₂S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₃H₁₇NO₂S

There total 2 articles about C₁₃H₁₇NO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C22H37NO2SSi → C13H17NO2S (1611453-98-5)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 1.5h;

DOI:10.1021/acs.joc.5b00222

Reference yield:

toluene-4-sulfonamide (70-55-3) → C13H17NO2S (1611453-98-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium sulfate; caesium carbonate; copper(II) bis(trifluoromethanesulfonate) / toluene / 48 h / 120 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 - 20 °C

With tetrabutyl ammonium fluoride; copper(II) bis(trifluoromethanesulfonate); caesium carbonate; sodium sulfate; In tetrahydrofuran; toluene;

DOI:10.1021/acs.joc.5b00222

Reference yield: 99.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + C13H17NO2S (1611453-98-5) → 2-(1-methylethyl)-1-(p-tolylsulfonyl)-2,5-dihydro-1H-pyrrole (138491-98-2)

Guidance literature:

With N-cyclohexyl-cyclohexanamine; copper(I) bromide; In 1,4-dioxane; at 180 ℃; for 5h; Microwave irradiation;

DOI:10.1002/ejoc.201301621

upstream raw materials:

toluene-4-sulfonamide

Downstream raw materials:

2-(1-methylethyl)-1-(p-tolylsulfonyl)-2,5-dihydro-1H-pyrrole

2-isopropyl-1-(toluene-4-sulfonyl)-1H-pyrrole