2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato oxovanadium(IV)

Base Information

Chemical Name:2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato oxovanadium(IV)
CAS No.:131214-94-3
Molecular Formula:C₄₄H₂₀Br₈N₄OV
Molecular Weight:1310.84
Hs Code.:

Synonyms:2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato oxovanadium(IV)

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Chemical Property of 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato oxovanadium(IV)

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Technology Process of 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato oxovanadium(IV)

There total 3 articles about 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato oxovanadium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 14705-63-6
oxovanadium(IV) tetraphenylporphyrin

: 7558-02-3,7758-02-3
potassium bromide

: 131214-94-3
2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato oxovanadium(IV)

Guidance literature:: With perchloric acid; dihydrogen peroxide; In dichloromethane; water; at 25 ℃; for 36h;
DOI:10.1002/ejic.202100116

Reference yield: 80.0%

: 3153-26-2
bis(acetylacetonate)oxovanadium

: 2,3,7,8,12,13,17,18-octobromo-5,10,15,20-tetraphenyl, 21H,23H-porphyrin

: 131214-94-3
2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato oxovanadium(IV)

Guidance literature:: In N,N-dimethyl-formamide; DMF soln. of educts were mixed, refluxed for 24h;; DMF was evapd. under reduced pressure, residue was dissolved in CHCl3, mixt. was washed with water, dried over Na2SO4; chromd. on basic alumina with CHCl3 as eluant, 1st moving fraction was collected, solvent was evapd.;

Reference yield:

: 14705-63-6
oxovanadium(IV) tetraphenylporphyrin

: 131214-94-3
2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato oxovanadium(IV)

Guidance literature:: With perchloric acid; dihydrogen peroxide; potassium bromide; In dichloromethane; water; at 20 ℃; for 36h;
DOI:10.1142/S108842462250002X