methyl-1-{[4-[4-(2S)-N-pyrrolidine-2-carboxaldehydediethyl thioacetal]butyl]-2-methoxy-5-nitrophenoxy}-2-(1-methyl-3-indolyl)benzimidazol-6-carboxylate

Base Information

Chemical Name:methyl-1-{[4-[4-(2S)-N-pyrrolidine-2-carboxaldehydediethyl thioacetal]butyl]-2-methoxy-5-nitrophenoxy}-2-(1-methyl-3-indolyl)benzimidazol-6-carboxylate
CAS No.:1467028-84-7
Molecular Formula:C₄₀H₄₇N₅O₇S₂
Molecular Weight:773.974
Hs Code.:

methyl-1-{[4-[4-(2S)-N-pyrrolidine-2-carboxaldehydediethyl thioacetal]butyl]-2-methoxy-5-nitrophenoxy}-2-(1-methyl-3-indolyl)benzimidazol-6-carboxylate

Synonyms:methyl-1-{[4-[4-(2S)-N-pyrrolidine-2-carboxaldehydediethyl thioacetal]butyl]-2-methoxy-5-nitrophenoxy}-2-(1-methyl-3-indolyl)benzimidazol-6-carboxylate

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Chemical Property of methyl-1-{[4-[4-(2S)-N-pyrrolidine-2-carboxaldehydediethyl thioacetal]butyl]-2-methoxy-5-nitrophenoxy}-2-(1-methyl-3-indolyl)benzimidazol-6-carboxylate

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Technology Process of methyl-1-{[4-[4-(2S)-N-pyrrolidine-2-carboxaldehydediethyl thioacetal]butyl]-2-methoxy-5-nitrophenoxy}-2-(1-methyl-3-indolyl)benzimidazol-6-carboxylate

There total 7 articles about methyl-1-{[4-[4-(2S)-N-pyrrolidine-2-carboxaldehydediethyl thioacetal]butyl]-2-methoxy-5-nitrophenoxy}-2-(1-methyl-3-indolyl)benzimidazol-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1467028-67-6
ethyl 2-(1-methyl-1H-indol-3-yl)-1H-1,3-benzodiazole-6-carboxylate

: 343308-56-5
(2S)-N-[4-(4-bromobutyl)oxy-5-methoxy-2-nitrobenzoyl]pyrrolidine-2-carboxaldehyde diethylthioacetal

: 1467028-84-7
methyl-1-{[4-[4-(2S)-N-pyrrolidine-2-carboxaldehydediethyl thioacetal]butyl]-2-methoxy-5-nitrophenoxy}-2-(1-methyl-3-indolyl)benzimidazol-6-carboxylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.2174/1573406411309050004

Reference yield:

: 19012-03-4
N-methyl-3-formylindole

: 1467028-84-7
methyl-1-{[4-[4-(2S)-N-pyrrolidine-2-carboxaldehydediethyl thioacetal]butyl]-2-methoxy-5-nitrophenoxy}-2-(1-methyl-3-indolyl)benzimidazol-6-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium metabisulfite / ethanol; water / 4 h

2: potassium carbonate / N,N-dimethyl-formamide / 48 h / 20 °C

With sodium metabisulfite; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.2174/1573406411309050004

Reference yield:

: 37466-90-3
ethyl 3,4-diaminobenzoate

: 1467028-84-7
methyl-1-{[4-[4-(2S)-N-pyrrolidine-2-carboxaldehydediethyl thioacetal]butyl]-2-methoxy-5-nitrophenoxy}-2-(1-methyl-3-indolyl)benzimidazol-6-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium metabisulfite / ethanol; water / 4 h

2: potassium carbonate / N,N-dimethyl-formamide / 48 h / 20 °C

With sodium metabisulfite; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.2174/1573406411309050004