5-chloro-2-<3-(hemisuccinaminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone

Base Information

Chemical Name:5-chloro-2-<3-(hemisuccinaminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone
CAS No.:102537-68-8
Molecular Formula:C₂₁H₁₉ClN₄O₄
Molecular Weight:426.859
Hs Code.:

Synonyms:5-chloro-2-<3-(hemisuccinaminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-chloro-2-<3-(hemisuccinaminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone

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Technology Process of 5-chloro-2-<3-(hemisuccinaminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone

There total 2 articles about 5-chloro-2-<3-(hemisuccinaminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 108-30-5
succinic acid anhydride

: 85966-74-1
({2-[3-(aminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl]-5-chlorophenyl}(phenyl)methanone)

: 102537-68-8
5-chloro-2-<3-(hemisuccinaminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; for 0.5h; Ambient temperature;
DOI:10.1021/jm00158a004

Reference yield:

: 28981-97-7
alprazolam

: 102537-68-8
5-chloro-2-<3-(hemisuccinaminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 0.33 N HCl

2: 27 percent / 1.0 N NaOH (pH 9.0) / tetrahydrofuran / 0.5 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; In tetrahydrofuran;
DOI:10.1021/jm00158a004