2,3-O-Benzyliden-1,4-di-O-<(Z)-2-formylamino-3-(2-thienyl)acryloyl>-L-threit

Base Information

Chemical Name:2,3-O-Benzyliden-1,4-di-O-<(Z)-2-formylamino-3-(2-thienyl)acryloyl>-L-threit
CAS No.:99371-41-2
Molecular Formula:C₂₇H₂₄N₂O₈S₂
Molecular Weight:568.628
Hs Code.:

Synonyms:2,3-O-Benzyliden-1,4-di-O-<(Z)-2-formylamino-3-(2-thienyl)acryloyl>-L-threit

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Chemical Property of 2,3-O-Benzyliden-1,4-di-O-<(Z)-2-formylamino-3-(2-thienyl)acryloyl>-L-threit

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Technology Process of 2,3-O-Benzyliden-1,4-di-O-<(Z)-2-formylamino-3-(2-thienyl)acryloyl>-L-threit

There total 3 articles about 2,3-O-Benzyliden-1,4-di-O-<(Z)-2-formylamino-3-(2-thienyl)acryloyl>-L-threit which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 94730-27-5
(4S,5S)-2-phenyl-4,5-di(methanesulphonyloxymethyl)-1,3-dioxolan

: 99371-32-1
(Z)-α-Formylamino-β-(2-thienyl)acrylsaeure

: 99371-41-2
2,3-O-Benzyliden-1,4-di-O-<(Z)-2-formylamino-3-(2-thienyl)acryloyl>-L-threit

Guidance literature:: With triethylamine; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 120 ℃; for 20h;

Reference yield:

: 98-03-3
thiophene-2-carbaldehyde

: 99371-41-2
2,3-O-Benzyliden-1,4-di-O-<(Z)-2-formylamino-3-(2-thienyl)acryloyl>-L-threit

Guidance literature:: Multi-step reaction with 3 steps

1: KOC(CH₃)3

2: 76 percent / 3 N KOH / tetrahydrofuran / 24 h / 20 °C

3: 62 percent / NEt₃ / hexamethylphosphoric acid triamide / 20 h / 120 °C

With potassium hydroxide; potassium tert-butylate; triethylamine; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;

Reference yield:

: 99371-33-2
(Z)-α-Formylamino-β-(2-thienyl)acrylsaeure-methylester

: 99371-41-2
2,3-O-Benzyliden-1,4-di-O-<(Z)-2-formylamino-3-(2-thienyl)acryloyl>-L-threit

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / 3 N KOH / tetrahydrofuran / 24 h / 20 °C

2: 62 percent / NEt₃ / hexamethylphosphoric acid triamide / 20 h / 120 °C

With potassium hydroxide; triethylamine; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;