(R)-2-(3-Azido-propyl)-2-((S)-2-methoxymethyl-pyrrolidine-1-carbonyl)-cyclohex-3-enone

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Chemical Name:(R)-2-(3-Azido-propyl)-2-((S)-2-methoxymethyl-pyrrolidine-1-carbonyl)-cyclohex-3-enone
CAS No.:171523-73-2
Molecular Formula:C₁₆H₂₄N₄O₃
Molecular Weight:320.392
Hs Code.:

Synonyms:(R)-2-(3-Azido-propyl)-2-((S)-2-methoxymethyl-pyrrolidine-1-carbonyl)-cyclohex-3-enone

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Chemical Property of (R)-2-(3-Azido-propyl)-2-((S)-2-methoxymethyl-pyrrolidine-1-carbonyl)-cyclohex-3-enone

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Technology Process of (R)-2-(3-Azido-propyl)-2-((S)-2-methoxymethyl-pyrrolidine-1-carbonyl)-cyclohex-3-enone

There total 2 articles about (R)-2-(3-Azido-propyl)-2-((S)-2-methoxymethyl-pyrrolidine-1-carbonyl)-cyclohex-3-enone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 171523-91-4
[(R)-1-(3-Azido-propyl)-2-methoxy-cyclohexa-2,5-dienyl]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-methanone

: 171523-73-2
(R)-2-(3-Azido-propyl)-2-((S)-2-methoxymethyl-pyrrolidine-1-carbonyl)-cyclohex-3-enone

Guidance literature:: With hydrogenchloride; In methanol; for 18h; Ambient temperature;
DOI:10.1021/jo00129a052

Reference yield:

: 102069-84-1
(S)-2-methoxy-1-[[2'-(methoxymethyl)pyrrolidinyl]carbonyl]benzene

: 171523-73-2
(R)-2-(3-Azido-propyl)-2-((S)-2-methoxymethyl-pyrrolidine-1-carbonyl)-cyclohex-3-enone

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / NH₃, K, t-BuOH, piperylene / tetrahydrofuran / -78 deg C, 30 min., -78 deg C, 3 h

2: 82 percent / 6N aq. HCl / methanol / 18 h / Ambient temperature

With hydrogenchloride; penta-1,3-diene; ammonia; tert-butyl alcohol; In tetrahydrofuran; methanol;
DOI:10.1021/jo00129a052

Reference yield: 88.0%

: 171523-73-2
(R)-2-(3-Azido-propyl)-2-((S)-2-methoxymethyl-pyrrolidine-1-carbonyl)-cyclohex-3-enone

: (2R,3R,4S)-2-(3-Azido-propyl)-3,4-dihydroxy-2-((S)-2-methoxymethyl-pyrrolidine-1-carbonyl)-cyclohexanone

Guidance literature:: With osmium(VIII) oxide; N-methyl-2-indolinone; In water; acetone; tert-butyl alcohol; for 48h; Ambient temperature;
DOI:10.1016/S0040-4039(98)01440-3