N-tert-butoxycarbonyl-3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester

Base Information

Chemical Name:N-tert-butoxycarbonyl-3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester
CAS No.:82071-44-1
Molecular Formula:C₂₉H₃₁NO₆
Molecular Weight:489.568
Hs Code.:

Synonyms:N-tert-butoxycarbonyl-3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester

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Chemical Property of N-tert-butoxycarbonyl-3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester

Chemical Property:

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Technology Process of N-tert-butoxycarbonyl-3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester

There total 3 articles about N-tert-butoxycarbonyl-3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 62631-41-8
N-tert-butoxycarbonyl-3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine

: 82071-44-1
N-tert-butoxycarbonyl-3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester

Guidance literature:: In diethyl ether; for 1h;
DOI:10.1248/cpb.30.474

Reference yield:

: 58632-95-4
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

: 82071-44-1
N-tert-butoxycarbonyl-3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 65.6 percent / Et₃N / dioxane; H₂O / 48 h / Ambient temperature

2: 98 percent / diethyl ether / 1 h

With triethylamine; In 1,4-dioxane; diethyl ether; water;
DOI:10.1248/cpb.30.474

Reference yield:

: 55943-50-5,56083-23-9
3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine hydrochloride

: 82071-44-1
N-tert-butoxycarbonyl-3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 65.6 percent / Et₃N / dioxane; H₂O / 48 h / Ambient temperature

2: 98 percent / diethyl ether / 1 h

With triethylamine; In 1,4-dioxane; diethyl ether; water;
DOI:10.1248/cpb.30.474