3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester hydrochloride

Base Information

Chemical Name:3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester hydrochloride
CAS No.:82071-45-2
Molecular Formula:C₂₄H₂₃NO₄*ClH
Molecular Weight:425.912
Hs Code.:

Synonyms:3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester hydrochloride

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Chemical Property of 3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester hydrochloride

Chemical Property:

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Technology Process of 3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester hydrochloride

There total 3 articles about 3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.3%

: 82071-44-1
N-tert-butoxycarbonyl-3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester

: 82071-45-2
3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester hydrochloride

Guidance literature:: With formic acid; In ethyl acetate; for 48h; Ambient temperature;
DOI:10.1248/cpb.30.474

Reference yield:

: 62631-41-8
N-tert-butoxycarbonyl-3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine

: 82071-45-2
3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / diethyl ether / 1 h

2: 96.3 percent / HCOOH / ethyl acetate / 48 h / Ambient temperature

With formic acid; In diethyl ether; ethyl acetate;
DOI:10.1248/cpb.30.474

Reference yield:

: 55943-50-5,56083-23-9
3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine hydrochloride

: 82071-45-2
3,4-diphenylmethylenedioxyphenyl-2-methyl-L-alanine methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 65.6 percent / Et₃N / dioxane; H₂O / 48 h / Ambient temperature

2: 98 percent / diethyl ether / 1 h

3: 96.3 percent / HCOOH / ethyl acetate / 48 h / Ambient temperature

With formic acid; triethylamine; In 1,4-dioxane; diethyl ether; water; ethyl acetate;
DOI:10.1248/cpb.30.474