Ethyl (2S,3S)-3-hydroxy-2-methyl-3-phenylpropionic acid

Base Information

Chemical Name:Ethyl (2S,3S)-3-hydroxy-2-methyl-3-phenylpropionic acid
CAS No.:155320-73-3
Molecular Formula:C₁₂H₁₆O₃
Molecular Weight:208.257
Hs Code.:

Synonyms:Ethyl (2S,3S)-3-hydroxy-2-methyl-3-phenylpropionic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl (2S,3S)-3-hydroxy-2-methyl-3-phenylpropionic acid

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Technology Process of Ethyl (2S,3S)-3-hydroxy-2-methyl-3-phenylpropionic acid

There total 21 articles about Ethyl (2S,3S)-3-hydroxy-2-methyl-3-phenylpropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 155189-52-9
ethyl (2S)-2-benzoylpropanate

: 155320-73-3
Ethyl (2S,3S)-3-hydroxy-2-methyl-3-phenylpropionic acid

Guidance literature:: With borane pyridine; titanium tetrachloride; In dichloromethane; at -78 ℃; for 0.166667h;
DOI:10.1021/jo00083a004

Reference yield:

: 10488-87-6
ethyl 2-benzoylpropionate

: 155320-73-3
Ethyl (2S,3S)-3-hydroxy-2-methyl-3-phenylpropionic acid

: ethyl 3-hydroxy-2-methyl-3-phenylpropanoate

: 189098-10-0
ethyl (2R,3R)-3-phenyl-3-hydroxy-2-methylpropionate

Guidance literature:: With D-glucose; In aq. phosphate buffer; at 28 ℃; for 24h; pH=7; Overall yield = 96 %; stereoselective reaction; Microbiological reaction;
DOI:10.1016/j.tetlet.2014.10.133

Reference yield:

: ethyl (3R)-2-bromo-3-hydroxy-2-methyl-3-phenylpropionate

: 155320-73-3
Ethyl (2S,3S)-3-hydroxy-2-methyl-3-phenylpropionic acid

: 192135-52-7
(2R,3S)-3-hydroxy-2-methyl-3-phenyl-propionic acid ethyl ester

Guidance literature:: With tri-n-butyl-tin hydride; magnesium bromide; triethyl borane; In dichloromethane; at 0 ℃; for 2.5h;
DOI:10.1246/bcsj.74.1485