4-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyloxy)-3-allylphenylbenzenamide

Base Information

Chemical Name:4-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyloxy)-3-allylphenylbenzenamide
CAS No.:1394965-65-1
Molecular Formula:C₃₁H₃₉NO₂
Molecular Weight:457.656
Hs Code.:

Synonyms:4-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyloxy)-3-allylphenylbenzenamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyloxy)-3-allylphenylbenzenamide

Chemical Property:

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Technology Process of 4-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyloxy)-3-allylphenylbenzenamide

There total 5 articles about 4-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyloxy)-3-allylphenylbenzenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 152974-10-2
C₁₆H₁₅NO₂

: 1394965-65-1
4-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyloxy)-3-allylphenylbenzenamide

Guidance literature:: With potassium carbonate; In acetone; for 12h; Reflux;
DOI:10.1016/j.bmc.2012.07.025

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1394965-65-1
4-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyloxy)-3-allylphenylbenzenamide

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / acetone / 16 h / Reflux

2: tin(II) chloride dihdyrate / ethanol / 0.33 h / Reflux; Inert atmosphere

3: chloroformic acid ethyl ester; triethylamine / chloroform / 0.75 h / 20 - 50 °C

4: N,N-diethylaniline; hydrogen / 6 h / 200 °C

5: potassium carbonate / acetone / 12 h / Reflux

With tin(II) chloride dihdyrate; hydrogen; chloroformic acid ethyl ester; potassium carbonate; triethylamine; N,N-diethylaniline; In ethanol; chloroform; acetone;
DOI:10.1016/j.bmc.2012.07.025

Reference yield:

: 1568-66-7
1-allyloxy-4-nitrobenzene

: 1394965-65-1
4-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyloxy)-3-allylphenylbenzenamide

Guidance literature:: Multi-step reaction with 4 steps

1: tin(II) chloride dihdyrate / ethanol / 0.33 h / Reflux; Inert atmosphere

2: chloroformic acid ethyl ester; triethylamine / chloroform / 0.75 h / 20 - 50 °C

3: N,N-diethylaniline; hydrogen / 6 h / 200 °C

4: potassium carbonate / acetone / 12 h / Reflux

With tin(II) chloride dihdyrate; hydrogen; chloroformic acid ethyl ester; potassium carbonate; triethylamine; N,N-diethylaniline; In ethanol; chloroform; acetone;
DOI:10.1016/j.bmc.2012.07.025