2-chloro-4-fluorobenzhydroxymoyl chloride

Base Information

Chemical Name:2-chloro-4-fluorobenzhydroxymoyl chloride
CAS No.:1076224-05-9
Molecular Formula:C₇H₄Cl₂FNO
Molecular Weight:208.019
Hs Code.:

Synonyms:2-chloro-4-fluorobenzhydroxymoyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-chloro-4-fluorobenzhydroxymoyl chloride

Chemical Property:

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Technology Process of 2-chloro-4-fluorobenzhydroxymoyl chloride

There total 2 articles about 2-chloro-4-fluorobenzhydroxymoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 890934-19-7
2-chloro-4-fluorobenzaldehyde oxime

: 1076224-05-9
2-chloro-4-fluorobenzhydroxymoyl chloride

Guidance literature:: With N-chloro-succinimide; In N,N-dimethyl-formamide; acetonitrile; at 20 ℃; for 18h;

Reference yield:

: 84194-36-5
2-chloro-4-fluorobenzaldehyde

: 1076224-05-9
2-chloro-4-fluorobenzhydroxymoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; triethylamine / N,N-dimethyl-formamide / 1 h / 20 °C

2: N-chloro-succinimide / N,N-dimethyl-formamide / 20 °C

With N-chloro-succinimide; hydroxylamine hydrochloride; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2011.05.104