ethyl N-geranyl-N-tosylcarbamate

Base Information

Chemical Name:ethyl N-geranyl-N-tosylcarbamate
CAS No.:124658-92-0
Molecular Formula:C₂₀H₂₉NO₄S
Molecular Weight:379.521
Hs Code.:

Synonyms:ethyl N-geranyl-N-tosylcarbamate

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Chemical Property of ethyl N-geranyl-N-tosylcarbamate

Chemical Property:

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Technology Process of ethyl N-geranyl-N-tosylcarbamate

There total 1 articles about ethyl N-geranyl-N-tosylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6138-90-5
trans-geranyl bromide

: 5577-13-9
Tosylurethane

: 124658-92-0
ethyl N-geranyl-N-tosylcarbamate

Guidance literature:: With sodium; Yield given. Multistep reaction; 1.) EtOH, RT; 0.5 h, 2.) EtOH, 1 h;
DOI:10.1246/bcsj.62.2050

Reference yield: 99.0%

: 124658-92-0
ethyl N-geranyl-N-tosylcarbamate

: 124658-85-1
(E)-N-(3,7-dimethylocta-2,6-dien-1-yl)-4-methylbenzenesulfonamide

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; water; for 12h;
DOI:10.1246/bcsj.62.2050

Reference yield:

: 124658-92-0
ethyl N-geranyl-N-tosylcarbamate

: 2-butoxy-4-(5-methyl-1-methylene-4-hexenyl)-1-tosylpyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / 50percent NaOH / tetrahydrofuran; H₂O; methanol / 12 h

2: 86 percent / Pd(OAc)2 / toluene / 2 h / 25 °C

With palladium diacetate; sodium hydroxide; In tetrahydrofuran; methanol; water; toluene;
DOI:10.1246/bcsj.62.2050