Ir((FC₆H₄)3P)2((CH₃)2C₆H₅)H⁽¹⁺⁾*SbF₆^(1-)=(Ir((FC₆H₄)3P)2(C₆H₅(CH₃)2H))SbF₆

Base Information

• Chemical Name: Ir((FC₆H₄)3P)2((CH₃)2C₆H₅)H⁽¹⁺⁾*SbF₆^(1-)=(Ir((FC₆H₄)3P)2(C₆H₅(CH₃)2H))SbF₆
• CAS No.: 94986-33-1
• Molecular Formula: C₄₄H₃₆F₆IrP₂*F₆Sb
• Molecular Weight: 1168.67

Synonyms:Ir((FC₆H₄)3P)2((CH₃)2C₆H₅)H⁽¹⁺⁾*SbF₆^(1-)=(Ir((FC₆H₄)3P)2(C₆H₅(CH₃)2H))SbF₆

Chemical Property of Ir((FC₆H₄)3P)2((CH₃)2C₆H₅)H⁽¹⁺⁾*SbF₆^(1-)=(Ir((FC₆H₄)3P)2(C₆H₅(CH₃)2H))SbF₆

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Technology Process of Ir((FC₆H₄)3P)2((CH₃)2C₆H₅)H⁽¹⁺⁾*SbF₆^(1-)=(Ir((FC₆H₄)3P)2(C₆H₅(CH₃)2H))SbF₆

There total 2 articles about Ir((FC₆H₄)3P)2((CH₃)2C₆H₅)H⁽¹⁺⁾*SbF₆^(1-)=(Ir((FC₆H₄)3P)2(C₆H₅(CH₃)2H))SbF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

dihydridobis(acetone)bis(tris(p-fluorophenyl)phosphine)iridium(III) hexafluoroantimonate (89529-62-4) + 1,1-dimethylcyclohexane (590-66-9) → Ir((FC6H4)3P)2((CH3)2C6H5)H(1+)*SbF6(1-)=(Ir((FC6H4)3P)2(C6H5(CH3)2H))SbF6 (94986-33-1)

Guidance literature:

With tert-butylethylene; In neat (no solvent); freeing from air by freeze-thaw cycling; heating for 24 h at 145°C; removal of volatiles in vac.; recrystn. from CH2Cl2/Et2O;

DOI:10.1021/ja00283a015

Reference yield:

dihydridobis(acetone)bis(tris(p-fluorophenyl)phosphine)iridium(III) hexafluoroantimonate (89529-62-4) + 6,6-dimethylcyclohexadiene (695-28-3) → Ir((FC6H4)3P)2((CH3)2C6H5)H(1+)*SbF6(1-)=(Ir((FC6H4)3P)2(C6H5(CH3)2H))SbF6 (94986-33-1)

Guidance literature:

In neat (no solvent); Ir complex heating with cyclodiene at 85°C for 2 h; identified by NMR and IR spectra;

DOI:10.1039/c39840001260

upstream raw materials:

dihydridobis(acetone)bis(tris(p-fluorophenyl)phosphine)iridium(III) hexafluoroantimonate

1,1-dimethylcyclohexane

6,6-dimethylcyclohexadiene

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