Boc-cyclohexylnorstatine isopropylamide

Base Information

Chemical Name:Boc-cyclohexylnorstatine isopropylamide
CAS No.:119600-98-5
Molecular Formula:C₁₈H₃₄N₂O₄
Molecular Weight:342.479
Hs Code.:

Synonyms:Boc-cyclohexylnorstatine isopropylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Boc-cyclohexylnorstatine isopropylamide

Chemical Property:

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Technology Process of Boc-cyclohexylnorstatine isopropylamide

There total 3 articles about Boc-cyclohexylnorstatine isopropylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 105116-44-7
N-Boc-cyclohexylnorstatin

: 75-31-0
isopropylamine

: 119600-98-5
Boc-cyclohexylnorstatine isopropylamide

Guidance literature:: With N-hydroxy-5-norbornene-2,3-dicarboximide; dicyclohexyl-carbodiimide; In ethyl acetate; Ambient temperature;
DOI:10.1248/cpb.38.2487

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 119600-98-5
Boc-cyclohexylnorstatine isopropylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / triethylamine / dioxane; H₂O / 2 h / 0 °C / 2) room temperature, overnight

2: 100 percent / N-hydroxy-5-norbornene-2,3-dicarboximide, dicyclohexylcarbodiimide / ethyl acetate / Ambient temperature

With N-hydroxy-5-norbornene-2,3-dicarboximide; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; water; ethyl acetate;
DOI:10.1248/cpb.38.2487

Reference yield:

: 121506-22-7
(2R,3S)-nor-C-statine hydrochloride

: 119600-98-5
Boc-cyclohexylnorstatine isopropylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / triethylamine / dioxane; H₂O / 2 h / 0 °C / 2) room temperature, overnight

2: 100 percent / N-hydroxy-5-norbornene-2,3-dicarboximide, dicyclohexylcarbodiimide / ethyl acetate / Ambient temperature

With N-hydroxy-5-norbornene-2,3-dicarboximide; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; water; ethyl acetate;
DOI:10.1248/cpb.38.2487