6-Amino-hexanoic acid [(S)-1-((S)-1-{(R)-1-[(S)-1-((S)-1-hydrazinocarbonyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butyl]-2-oxo-pyrrolidin-3-ylcarbamoyl}-2-phenyl-ethylcarbamoyl)-2-phenyl-ethyl]-amide

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Chemical Name:6-Amino-hexanoic acid [(S)-1-((S)-1-{(R)-1-[(S)-1-((S)-1-hydrazinocarbonyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butyl]-2-oxo-pyrrolidin-3-ylcarbamoyl}-2-phenyl-ethylcarbamoyl)-2-phenyl-ethyl]-amide
CAS No.:1026617-74-2
Molecular Formula:C₃₉H₅₈N₈O₆S
Molecular Weight:767.006
Hs Code.:

6-Amino-hexanoic acid [(S)-1-((S)-1-{(R)-1-[(S)-1-((S)-1-hydrazinocarbonyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butyl]-2-oxo-pyrrolidin-3-ylcarbamoyl}-2-phenyl-ethylcarbamoyl)-2-phenyl-ethyl]-amide

Synonyms:6-Amino-hexanoic acid [(S)-1-((S)-1-{(R)-1-[(S)-1-((S)-1-hydrazinocarbonyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butyl]-2-oxo-pyrrolidin-3-ylcarbamoyl}-2-phenyl-ethylcarbamoyl)-2-phenyl-ethyl]-amide

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Chemical Property of 6-Amino-hexanoic acid [(S)-1-((S)-1-{(R)-1-[(S)-1-((S)-1-hydrazinocarbonyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butyl]-2-oxo-pyrrolidin-3-ylcarbamoyl}-2-phenyl-ethylcarbamoyl)-2-phenyl-ethyl]-amide

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Technology Process of 6-Amino-hexanoic acid [(S)-1-((S)-1-{(R)-1-[(S)-1-((S)-1-hydrazinocarbonyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butyl]-2-oxo-pyrrolidin-3-ylcarbamoyl}-2-phenyl-ethylcarbamoyl)-2-phenyl-ethyl]-amide

There total 2 articles about 6-Amino-hexanoic acid [(S)-1-((S)-1-{(R)-1-[(S)-1-((S)-1-hydrazinocarbonyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butyl]-2-oxo-pyrrolidin-3-ylcarbamoyl}-2-phenyl-ethylcarbamoyl)-2-phenyl-ethyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [(R)-3-tert-Butoxycarbonylamino-3-((S)-1-methoxycarbonyl-3-methyl-butylcarbamoyl)-propyl]-dimethyl-sulfonium; iodide

: 1026617-74-2
6-Amino-hexanoic acid [(S)-1-((S)-1-{(R)-1-[(S)-1-((S)-1-hydrazinocarbonyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butyl]-2-oxo-pyrrolidin-3-ylcarbamoyl}-2-phenyl-ethylcarbamoyl)-2-phenyl-ethyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylformamide; CH₂Cl₂ / 2 h / 0 °C

With sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00053a001

Reference yield:

: 70604-37-4
L'anhydride symetrique de l'acide ε-aminocaproique N-t-BOC protege

: 75530-96-0
(Fmoc-Phe-O)2O

: 82611-48-1
(2S)-2-<(3R)-3-<(tert-butoxycarbonyl)amino>-2-oxopyrrolidin-1-yl>-4-methylpentanoic acid

: C₄₀H₄₀N₂O₇S₂

: 1026617-74-2
6-Amino-hexanoic acid [(S)-1-((S)-1-{(R)-1-[(S)-1-((S)-1-hydrazinocarbonyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butyl]-2-oxo-pyrrolidin-3-ylcarbamoyl}-2-phenyl-ethylcarbamoyl)-2-phenyl-ethyl]-amide

Guidance literature:: Multistep reaction;
DOI:10.1021/jm00053a001

Reference yield:

: 1026617-74-2
6-Amino-hexanoic acid [(S)-1-((S)-1-{(R)-1-[(S)-1-((S)-1-hydrazinocarbonyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butyl]-2-oxo-pyrrolidin-3-ylcarbamoyl}-2-phenyl-ethylcarbamoyl)-2-phenyl-ethyl]-amide

: (S)-2-[(S)-2-((R)-3-{(S)-2-[(S)-2-(6-Amino-hexanoylamino)-3-phenyl-propionylamino]-3-phenyl-propionylamino}-2-oxo-pyrrolidin-1-yl)-4-methyl-pentanoylamino]-4-methylsulfanyl-butyryl azide; hydrochloride

Guidance literature:: With hydrogenchloride; isopentyl nitrite; In tetrahydrofuran; N,N-dimethyl-formamide; at -20 ℃; for 4h;
DOI:10.1021/jm00053a001