L'anhydride symetrique de l'acide ε-aminocaproique N-t-BOC protege

Base Information

Chemical Name:L'anhydride symetrique de l'acide ε-aminocaproique N-t-BOC protege
CAS No.:70604-37-4
Molecular Formula:C₂₂H₄₀N₂O₇
Molecular Weight:444.569
Hs Code.:

Synonyms:L'anhydride symetrique de l'acide ε-aminocaproique N-t-BOC protege

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Chemical Property of L'anhydride symetrique de l'acide ε-aminocaproique N-t-BOC protege

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Technology Process of L'anhydride symetrique de l'acide ε-aminocaproique N-t-BOC protege

There total 1 articles about L'anhydride symetrique de l'acide ε-aminocaproique N-t-BOC protege which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6404-29-1
6-(tert-butoxycarbonylamino)hexanoic acid

: 70604-37-4
L'anhydride symetrique de l'acide ε-aminocaproique N-t-BOC protege

Guidance literature:: With dicyclohexyl-carbodiimide;

Reference yield:

: 70604-37-4
L'anhydride symetrique de l'acide ε-aminocaproique N-t-BOC protege

: (2S,5S,15S,18S,21R)-15,18-Dibenzyl-2-isobutyl-5-(2-methylsulfanyl-ethyl)-1,4,7,14,17,20-hexaaza-bicyclo[19.2.1]tetracosane-3,6,13,16,19,24-hexaone

Guidance literature:: Multi-step reaction with 3 steps

2: 4.2 M HCl, isopentyl nitrite / dimethylformamide; tetrahydrofuran / 4 h / -20 °C

3: Et₃N / dimethylformamide / 20 h / -25 °C

With hydrogenchloride; triethylamine; isopentyl nitrite; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00053a001

Reference yield:

: 70604-37-4
L'anhydride symetrique de l'acide ε-aminocaproique N-t-BOC protege

: (S)-2-[(S)-2-((R)-3-{(S)-2-[(S)-2-(6-Amino-hexanoylamino)-3-phenyl-propionylamino]-3-phenyl-propionylamino}-2-oxo-pyrrolidin-1-yl)-4-methyl-pentanoylamino]-4-methylsulfanyl-butyryl azide; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

2: 4.2 M HCl, isopentyl nitrite / dimethylformamide; tetrahydrofuran / 4 h / -20 °C

With hydrogenchloride; isopentyl nitrite; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00053a001