3-Methyl-8-oxo-7-(2-phenylacetamido)-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid,p-nitrobenzyl ester

Base Information

Chemical Name:3-Methyl-8-oxo-7-(2-phenylacetamido)-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid,p-nitrobenzyl ester
CAS No.:34104-27-3
Molecular Formula:C₂₃H₂₁N₃O₆S
Molecular Weight:467.502
Hs Code.:

Synonyms:3-Methyl-8-oxo-7-(2-phenylacetamido)-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid,p-nitrobenzyl ester

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Chemical Property of 3-Methyl-8-oxo-7-(2-phenylacetamido)-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid,p-nitrobenzyl ester

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Technology Process of 3-Methyl-8-oxo-7-(2-phenylacetamido)-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid,p-nitrobenzyl ester

There total 11 articles about 3-Methyl-8-oxo-7-(2-phenylacetamido)-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid,p-nitrobenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 34708-38-8
Potassium; 3-methyl-8-oxo-7-phenylacetylamino-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylate

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 34104-27-3
3-Methyl-8-oxo-7-(2-phenylacetamido)-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid,p-nitrobenzyl ester

Guidance literature:: 18-crown-6 ether; In acetonitrile; for 24h; Ambient temperature;
DOI:10.1055/s-1986-31474

Reference yield:

: 51415-43-1
10-chloro-6β-(2-phenoxy-acetylamino)-penicillanic acid 4-nitro-benzyl ester

: 34104-27-3
(6R)-3-methyl-8-oxo-7c-(2-phenyl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid 4-nitro-benzyl ester

Guidance literature:: With silver(I) acetate; In acetic acid;
DOI:10.1021/ja00844a045

Reference yield:

: 51415-20-4
(6R)-3-methyl-8-oxo-7t-phthalimido-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid 4-nitro-benzyl ester

: 34104-27-3
(6R)-3-methyl-8-oxo-7c-(2-phenyl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid 4-nitro-benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Na₂S*9H₂O / acetone; H₂O

2: DCC

3: (i) N₂H₄, THF, (ii) /BRN= 742254/

With sodium sulfide; dicyclohexyl-carbodiimide; In water; acetone;
DOI:10.1021/ja00852a044