3-(benzyloxycarbonylamino)propyl 4-O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:3-(benzyloxycarbonylamino)propyl 4-O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside
CAS No.:1334630-73-7
Molecular Formula:C₅₇H₆₆N₂O₁₄Si
Molecular Weight:1031.24
Hs Code.:

3-(benzyloxycarbonylamino)propyl 4-O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Synonyms:3-(benzyloxycarbonylamino)propyl 4-O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Chemical Property of 3-(benzyloxycarbonylamino)propyl 4-O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Technology Process of 3-(benzyloxycarbonylamino)propyl 4-O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

There total 4 articles about 3-(benzyloxycarbonylamino)propyl 4-O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₄H₆₂N₂O₁₄Si

: 77-76-9
2,2-dimethoxy-propane

: 1334630-73-7
3-(benzyloxycarbonylamino)propyl 4-O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.carres.2011.07.002

Reference yield:

: 107855-14-1
ethyl 2,3,4-tri-O-acetyl-6-O-benzyl-1-thio-β-D-galactopyranoside

: 1334630-73-7
3-(benzyloxycarbonylamino)propyl 4-O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve

1.2: 0.5 h / -40 °C / Inert atmosphere; Molecular sieve

2.1: sodium methylate / methanol / 0.5 h / 20 °C / Inert atmosphere

2.2: Amberlite-IR 120 (H+) / Inert atmosphere

3.1: camphor-10-sulfonic acid / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

With camphor-10-sulfonic acid; sodium methylate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2011.07.002

Reference yield:

: 347391-77-9
3-benzyloxycarbonylamino-1-propyl 6-O-tert-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 1334630-73-7
3-(benzyloxycarbonylamino)propyl 4-O-(6-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve

1.2: 0.5 h / -40 °C / Inert atmosphere; Molecular sieve

2.1: sodium methylate / methanol / 0.5 h / 20 °C / Inert atmosphere

2.2: Amberlite-IR 120 (H+) / Inert atmosphere

3.1: camphor-10-sulfonic acid / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

With camphor-10-sulfonic acid; sodium methylate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2011.07.002