benzyl N-[(1S)-1-(1H-1,2,3-benzotriazol-1-ylcarbonyl)-3-(methylsulfanyl)propyl]carbamate

Base Information

• Chemical Name: benzyl N-[(1S)-1-(1H-1,2,3-benzotriazol-1-ylcarbonyl)-3-(methylsulfanyl)propyl]carbamate
• CAS No.: 869772-05-4
• Molecular Formula: C₁₉H₂₀N₄O₃S
• Molecular Weight: 384.459

Synonyms:benzyl N-[(1S)-1-(1H-1,2,3-benzotriazol-1-ylcarbonyl)-3-(methylsulfanyl)propyl]carbamate

Chemical Property of benzyl N-[(1S)-1-(1H-1,2,3-benzotriazol-1-ylcarbonyl)-3-(methylsulfanyl)propyl]carbamate

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Technology Process of benzyl N-[(1S)-1-(1H-1,2,3-benzotriazol-1-ylcarbonyl)-3-(methylsulfanyl)propyl]carbamate

There total 1 articles about benzyl N-[(1S)-1-(1H-1,2,3-benzotriazol-1-ylcarbonyl)-3-(methylsulfanyl)propyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1,2,3-Benzotriazole (95-14-7,27556-51-0) + Cbz-Met-OH (1152-62-1) → benzyl N-[(1S)-1-(1H-1,2,3-benzotriazol-1-ylcarbonyl)-3-(methylsulfanyl)propyl]carbamate (869772-05-4)

Guidance literature:

1,2,3-Benzotriazole; With thionyl chloride; In tetrahydrofuran; at 25 ℃; for 0.5h; Inert atmosphere;

Cbz-Met-OH; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jo1015757

Reference yield: 95.0%

benzyl N-[(1S)-1-(1H-1,2,3-benzotriazol-1-ylcarbonyl)-3-(methylsulfanyl)propyl]carbamate (869772-05-4) + L-methionine (63-68-3,26062-47-5,58576-49-1) → (S)-2-[(S)-2-benzyloxycarbonylamino-4-methylsulfanylbutyrylamino]-3-methylsulfanylbutanoic acid (61413-48-7)

Guidance literature:

With triethylamine; In water; acetonitrile; at 20 ℃; for 1h;

DOI:10.1055/s-2006-926287

Reference yield: 95.0%

benzyl N-[(1S)-1-(1H-1,2,3-benzotriazol-1-ylcarbonyl)-3-(methylsulfanyl)propyl]carbamate (869772-05-4) + L-alanin (56-41-7,25191-17-7,18875-37-1) → (S)-2-[(S)-2-benzyloxycarbonylamino-4-methylsulfanylbutyrylamino]propanoic acid (24787-85-7)

Guidance literature:

With triethylamine; In water; acetonitrile; at 20 ℃; for 1h;

DOI:10.1055/s-2006-926287

upstream raw materials:

1,2,3-Benzotriazole

Cbz-Met-OH

Downstream raw materials:

(S)-2-[(S)-2-benzyloxycarbonylamino-4-methylsulfanylbutyrylamino]propanoic acid

(R)-2-[(S)-2-benzyloxycarbonylamino-4-methylsulfanylbytyrylamino]propanoic acid

(S)-2-[(S)-2-benzyloxycarbonylamino-4-methylsulfanylbutyrylamino]-3-methylsulfanylbutanoic acid

(2S)-2-{[(2S)-2-{[(benzyloxy)carbonyl]amino}-4-(methylsulfanyl)butanoyl]amino}pentanedioic acid

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